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MassMS-NW-0463 o-anisidine C7H9NO (Mass of molecular ion: 123)
Source Temperature: 240 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.8 18.0 2.2 26.0 1.3 27.0 4.5 28.0 5.2 37.0 1.3 38.0 3.0 39.0 8.5 40.0 1.2 41.0 3.0 42.0 1.2 43.0 1.0 50.0 3.3 51.0 6.2 52.0 10.8 53.0 15.2 54.0 3.2 62.0 1.4 63.0 3.3 64.0 1.8 65.0 10.4 66.0 2.2 77.0 2.8 78.0 2.6 79.0 2.1 80.0 65.8 81.0 4.4 91.0 1.5 92.0 5.6 93.0 2.1 94.0 2.1 105.0 2.7 106.0 1.4 108.0 98.1 109.0 7.5 122.0 1.2 123.0 100.0 124.0 8.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H9 N O 0.05 ml : 0.5 ml CDCl3 o-anisidine 
Assign. Shift(ppm)
A 6.76 B 6.74 C 6.700 D 6.653 E 3.769 F 3.7
Hz ppm Int.2710.69 6.783 66 2708.86 6.779 76 2703.49 6.765 153 2701.78 6.761 185 2700.20 6.757 90 2698.36 6.752 115 2696.41 6.747 97 2694.58 6.743 210 2692.02 6.736 242 2690.55 6.733 131 2683.59 6.715 161 2681.76 6.711 188 2676.51 6.698 114 2674.93 6.694 105 2673.71 6.691 84 2668.46 6.677 55 2666.75 6.673 58 2662.84 6.663 206 2661.01 6.659 145 2655.40 6.645 146 2653.81 6.641 114 1506.47 3.770 1000 1497.19 3.747 48
in CDCl3
CCl4 solution
liquid film
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