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MassMS-NW-0461 o-toluidine C7H9N (Mass of molecular ion: 107)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 2.9 28.0 4.1 30.0 2.0 38.0 2.0 39.0 6.6 40.0 1.2 41.0 2.1 42.0 1.6 50.0 3.5 51.0 6.5 52.0 5.4 52.5 1.6 53.0 5.9 53.5 3.0 54.0 2.2 62.0 1.2 63.0 2.8 64.0 1.5 65.0 2.8 66.0 1.4 77.0 14.3 78.0 5.2 79.0 11.7 80.0 4.3 89.0 6.1 90.0 5.7 91.0 3.6 104.0 2.5 105.0 1.0 106.0 97.7 107.0 100.0 108.0 7.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H9 N 0.05 ml : 0.5 ml CDCl3 o-toluidine 
Assign. Shift(ppm)
A 7.01 B 7.00 C 6.676 D 6.586 E 3.48 F 2.090
Hz ppm Int.2804.32 7.017 287 2803.71 7.016 304 2802.98 7.014 213 2796.88 6.999 373 2796.39 6.998 373 2789.92 6.981 115 2789.43 6.980 121 2788.33 6.977 92 2787.84 6.976 81 2675.29 6.695 123 2674.32 6.692 132 2668.09 6.677 196 2666.99 6.674 220 2660.52 6.658 98 2659.55 6.655 106 2636.47 6.597 189 2635.50 6.595 204 2633.91 6.591 82 2628.42 6.577 189 2627.20 6.574 152 1390.50 3.480 128 835.57 2.091 1000
in CDCl3
CCl4 solution
liquid film
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