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MS-NW-0570 N,N-dimethylaniline C8H11N (Mass of molecular ion: 121)
Source Temperature: 270 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 2.6 27.0 1.6 28.0 1.4 38.0 1.2 39.0 4.7 42.0 7.4 44.0 3.2 50.0 3.6 51.0 9.8 52.0 2.8 60.0 1.3 60.5 2.8 63.0 2.3 64.0 1.3 65.0 2.4 74.0 1.0 77.0 20.4 78.0 5.3 79.0 4.4 91.0 4.2 92.0 1.9 93.0 1.3 103.0 2.2 104.0 9.7 105.0 12.2 106.0 3.7 118.0 3.1 119.0 1.5 120.0 100.0 121.0 78.3 122.0 6.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H11 N 10.4 mol% in CDCl3 N,N-dimethylaniline Assign. Shift(ppm)
A 2.891 B 6.61 to 6.82 C 7.21
Hz ppm Int.
655.31 7.317 36 654.63 7.310 35 649.06 7.248 35 647.88 7.235 59 646.88 7.223 67 645.75 7.211 66 645.25 7.205 35 639.81 7.144 53 639.25 7.138 68 638.75 7.133 76 607.81 6.787 94 607.00 6.778 113 604.13 6.746 30 600.56 6.706 93 598.75 6.686 62 597.63 6.673 53 593.50 6.627 24 258.94 2.892 1000
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