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网站主页CAS数据库列表 367-25-9更多图谱2,4-二氟苯胺(367-25-9)红外图谱(IR)

2,4-二氟苯胺

产品名称 2,4-二氟苯胺

CAS号367-25-9

分子式C6H5F2N

分子量129.11

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  • Mass

    MS-IW-9511          
    2,4-difluoroaniline
    C6H5F2N             (Mass of molecular ion:    129)
    

       Source Temperature: 200 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          28.0       8.6
          31.0       3.8
          38.0       1.2
          50.0       2.0
          51.0       4.7
          52.0       4.0
          56.0       1.9
          57.0       4.3
          61.0       1.3
          62.0       2.4
          63.0       3.4
          64.5       4.5
          65.0       1.0
          75.0       4.2
          76.0       1.7
          81.0       4.4
          82.0      17.8
          83.0       3.4
          89.0       2.7
          98.0       1.0
          99.0       1.3
         100.0       1.5
         101.0      24.3
         102.0      20.8
         103.0       1.8
         108.0       2.7
         109.0      11.1
         110.0       1.2
         128.0       5.7
         129.0     100.0
         130.0       7.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H5 F2 N 0.05 ml : 0.5 ml CDCl3
    2,4-difluoroaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.754 B 6.67 C 3.59

         Hz     ppm     Int.
    

       2710.82   6.783    285
       2709.72   6.781    320
       2708.86   6.779    295
       2707.76   6.776    297
       2702.15   6.762    312
       2701.29   6.760    334
       2699.83   6.756    526
       2699.10   6.754    554
       2697.27   6.750    344
       2696.66   6.748    331
       2691.04   6.734    282
       2690.19   6.732    286
       2688.84   6.728    326
       2687.99   6.726    316
       2676.39   6.697    128
       2673.95   6.691    102
       2671.39   6.685    192
       2669.92   6.681    917
       2668.82   6.678    666
       2667.72   6.676    873
       2665.28   6.670    508
       2663.57   6.665   1000
       2662.72   6.663    977
       2659.91   6.656    774
       2657.59   6.650    869
       2656.74   6.648    561
       2654.79   6.643    155
       2654.05   6.641    131
       2651.25   6.634     86
       2648.80   6.628     79
       1436.04   3.594    205
    

in CDCl3