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MassMS-IW-9511 2,4-difluoroaniline C6H5F2N (Mass of molecular ion: 129)
Source Temperature: 200 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 8.6 31.0 3.8 38.0 1.2 50.0 2.0 51.0 4.7 52.0 4.0 56.0 1.9 57.0 4.3 61.0 1.3 62.0 2.4 63.0 3.4 64.5 4.5 65.0 1.0 75.0 4.2 76.0 1.7 81.0 4.4 82.0 17.8 83.0 3.4 89.0 2.7 98.0 1.0 99.0 1.3 100.0 1.5 101.0 24.3 102.0 20.8 103.0 1.8 108.0 2.7 109.0 11.1 110.0 1.2 128.0 5.7 129.0 100.0 130.0 7.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H5 F2 N 0.05 ml : 0.5 ml CDCl3 2,4-difluoroaniline 
Assign. Shift(ppm)
A 6.754 B 6.67 C 3.59
Hz ppm Int.2710.82 6.783 285 2709.72 6.781 320 2708.86 6.779 295 2707.76 6.776 297 2702.15 6.762 312 2701.29 6.760 334 2699.83 6.756 526 2699.10 6.754 554 2697.27 6.750 344 2696.66 6.748 331 2691.04 6.734 282 2690.19 6.732 286 2688.84 6.728 326 2687.99 6.726 316 2676.39 6.697 128 2673.95 6.691 102 2671.39 6.685 192 2669.92 6.681 917 2668.82 6.678 666 2667.72 6.676 873 2665.28 6.670 508 2663.57 6.665 1000 2662.72 6.663 977 2659.91 6.656 774 2657.59 6.650 869 2656.74 6.648 561 2654.79 6.643 155 2654.05 6.641 131 2651.25 6.634 86 2648.80 6.628 79 1436.04 3.594 205
in CDCl3
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