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甲基苯基二甲氧基硅烷

产品名称 甲基苯基二甲氧基硅烷

CAS号3027-21-2

分子式C9H14O2Si

分子量182.29

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  • Mass

    MS-IW-7190          
    dimethoxymethylphenylsilane
    C9H14O2Si           (Mass of molecular ion:    182)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          43.0       1.6
          45.0       2.7
          51.0       1.5
          59.0       9.6
          74.0       1.3
          75.0       6.8
          77.0       1.5
          78.0       1.1
          83.5       1.5
          91.0      15.4
          92.0       1.4
         104.0       1.0
         105.0       7.4
         107.0       7.8
         121.0       5.0
         137.0      28.4
         138.0       3.7
         139.0       1.2
         151.0       3.6
         167.0     100.0
         168.0      14.0
         169.0       4.6
         182.0      11.9
         183.0       1.8
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H14 O2 Si 0.05 ml : 0.5 ml CDCl3
    dimethoxymethylphenylsilane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.619 B 7.41 C 7.37 D 3.555 E 0.350 CONFIRMED BY LAOCN PROGRAM

         Hz     ppm     Int.
    

       3049.32   7.630    120
       3047.73   7.626    139
       3046.39   7.623     69
       3045.78   7.622     54
       3043.70   7.616     51
       3042.60   7.614     55
       3041.75   7.612    128
       3039.79   7.607    136
       2962.40   7.413     57
       2961.91   7.412     64
       2959.11   7.405     37
       2957.28   7.400     74
       2955.44   7.396    122
       2953.61   7.391    152
       2953.13   7.390    137
       2952.39   7.388     90
       2951.54   7.386     80
       2948.36   7.378     55
       2947.39   7.375     74
       2946.66   7.374     75
       2946.04   7.372    121
       2945.43   7.371     98
       2944.46   7.368     41
       2939.82   7.356     49
       2937.26   7.350     31
       1422.73   3.560    192
       1420.78   3.556   1000
       1418.70   3.550    170
        143.55   0.360     55
        140.01   0.351    719
        136.35   0.342     50
    

in CDCl3



liquid film