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MS-IW-7190 dimethoxymethylphenylsilane C9H14O2Si (Mass of molecular ion: 182)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
43.0 1.6 45.0 2.7 51.0 1.5 59.0 9.6 74.0 1.3 75.0 6.8 77.0 1.5 78.0 1.1 83.5 1.5 91.0 15.4 92.0 1.4 104.0 1.0 105.0 7.4 107.0 7.8 121.0 5.0 137.0 28.4 138.0 3.7 139.0 1.2 151.0 3.6 167.0 100.0 168.0 14.0 169.0 4.6 182.0 11.9 183.0 1.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H14 O2 Si 0.05 ml : 0.5 ml CDCl3 dimethoxymethylphenylsilane Assign. Shift(ppm)
A 7.619 B 7.41 C 7.37 D 3.555 E 0.350 CONFIRMED BY LAOCN PROGRAM
Hz ppm Int.
3049.32 7.630 120 3047.73 7.626 139 3046.39 7.623 69 3045.78 7.622 54 3043.70 7.616 51 3042.60 7.614 55 3041.75 7.612 128 3039.79 7.607 136 2962.40 7.413 57 2961.91 7.412 64 2959.11 7.405 37 2957.28 7.400 74 2955.44 7.396 122 2953.61 7.391 152 2953.13 7.390 137 2952.39 7.388 90 2951.54 7.386 80 2948.36 7.378 55 2947.39 7.375 74 2946.66 7.374 75 2946.04 7.372 121 2945.43 7.371 98 2944.46 7.368 41 2939.82 7.356 49 2937.26 7.350 31 1422.73 3.560 192 1420.78 3.556 1000 1418.70 3.550 170 143.55 0.360 55 140.01 0.351 719 136.35 0.342 50
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