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MS-IW-8605 dimethoxy(methyl)silane C3H10O2Si (Mass of molecular ion: 106)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 2.8 28.0 1.6 29.0 1.8 31.0 1.5 42.0 1.0 43.0 3.6 44.0 1.1 45.0 18.8 46.0 1.3 47.0 2.2 52.0 3.6 59.0 21.6 60.0 3.5 61.0 49.3 62.0 3.2 63.0 1.9 74.0 1.5 75.0 53.1 76.0 4.0 77.0 2.1 90.0 2.1 91.0 97.8 92.0 7.9 93.0 4.2 105.0 100.0 106.0 8.8 107.0 4.2 121.0 8.3 151.0 1.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C3 H10 O2 Si 0.05 ml : 0.5 ml CDCl3 dimethoxy(methyl)silane Assign. Shift(ppm)
A 4.532 B 3.562 C 0.193
Hz ppm Int.
1813.60 4.538 77 1812.01 4.534 182 1810.30 4.530 174 1808.59 4.526 67 1493.77 3.738 26 1436.28 3.594 22 1432.50 3.585 53 1423.58 3.563 1000 1415.77 3.543 53 1351.07 3.381 23 81.79 0.205 60 80.08 0.201 99 78.25 0.196 665 76.42 0.192 624 74.34 0.187 69 72.63 0.182 48
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