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MassMS-IW-9126 (3-chloropropyl)dimethoxy(methyl)silane C6H15ClO2Si (Mass of molecular ion: 182)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.2 28.0 1.3 29.0 1.1 31.0 1.1 39.0 1.9 41.0 5.4 42.0 42.8 43.0 3.3 45.0 7.0 58.0 1.0 59.0 11.6 60.0 1.4 61.0 2.9 74.0 2.1 75.0 36.3 76.0 2.8 77.0 1.6 79.0 4.3 81.0 1.8 91.0 2.1 95.0 10.2 97.0 3.7 105.0 100.0 106.0 8.6 107.0 4.1 109.0 11.9 110.0 1.0 111.0 4.4 121.0 3.8 125.0 30.7 126.0 2.3 127.0 11.0 139.0 6.1 140.0 1.0 141.0 12.6 142.0 1.2 143.0 3.9 167.0 1.3 169.0 1.2 199.0 2.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H15 Cl O2 Si 0.05 ml : 0.5 ml CDCl3 (3-chloropropyl)dimethoxy(methyl)silane 
Assign. Shift(ppm)
A 2.524 B 2.521 C 1.844 D 0.744 E 0.131
Hz ppm Int.1415.04 3.541 178 1409.30 3.527 305 1407.47 3.522 1000 1405.40 3.517 203 1404.54 3.515 108 1401.37 3.507 169 1400.76 3.505 125 752.32 1.883 47 745.48 1.866 90 744.26 1.863 38 743.53 1.861 35 740.72 1.854 50 739.99 1.852 55 738.65 1.849 53 737.55 1.846 59 736.69 1.844 60 735.47 1.841 57 733.89 1.837 53 733.15 1.835 52 730.71 1.829 33 729.86 1.827 35 728.64 1.824 99 721.80 1.807 49 305.30 0.764 120 300.17 0.752 52 296.63 0.743 81 293.70 0.735 51 288.45 0.722 110 56.03 0.141 54 54.93 0.138 79 52.61 0.132 616 49.07 0.123 54 48.34 0.121 65
in CDCl3
liquid film
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