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网站主页CAS数据库列表 18171-19-2更多图谱3-氯丙基甲基二甲氧基硅烷(18171-19-2)核磁图(1HNMR)

3-氯丙基甲基二甲氧基硅烷

产品名称 3-氯丙基甲基二甲氧基硅烷

CAS号18171-19-2

分子式C6H15ClO2Si

分子量182.72

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  • Mass

    MS-IW-9126          
    (3-chloropropyl)dimethoxy(methyl)silane
    C6H15ClO2Si         (Mass of molecular ion:    182)
    

       Source Temperature: 210 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       1.2
          28.0       1.3
          29.0       1.1
          31.0       1.1
          39.0       1.9
          41.0       5.4
          42.0      42.8
          43.0       3.3
          45.0       7.0
          58.0       1.0
          59.0      11.6
          60.0       1.4
          61.0       2.9
          74.0       2.1
          75.0      36.3
          76.0       2.8
          77.0       1.6
          79.0       4.3
          81.0       1.8
          91.0       2.1
          95.0      10.2
          97.0       3.7
         105.0     100.0
         106.0       8.6
         107.0       4.1
         109.0      11.9
         110.0       1.0
         111.0       4.4
         121.0       3.8
         125.0      30.7
         126.0       2.3
         127.0      11.0
         139.0       6.1
         140.0       1.0
         141.0      12.6
         142.0       1.2
         143.0       3.9
         167.0       1.3
         169.0       1.2
         199.0       2.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H15 Cl O2 Si 0.05 ml : 0.5 ml CDCl3
    (3-chloropropyl)dimethoxy(methyl)silane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.524 B 2.521 C 1.844 D 0.744 E 0.131

         Hz     ppm     Int.
    

       1415.04   3.541    178
       1409.30   3.527    305
       1407.47   3.522   1000
       1405.40   3.517    203
       1404.54   3.515    108
       1401.37   3.507    169
       1400.76   3.505    125
        752.32   1.883     47
        745.48   1.866     90
        744.26   1.863     38
        743.53   1.861     35
        740.72   1.854     50
        739.99   1.852     55
        738.65   1.849     53
        737.55   1.846     59
        736.69   1.844     60
        735.47   1.841     57
        733.89   1.837     53
        733.15   1.835     52
        730.71   1.829     33
        729.86   1.827     35
        728.64   1.824     99
        721.80   1.807     49
        305.30   0.764    120
        300.17   0.752     52
        296.63   0.743     81
        293.70   0.735     51
        288.45   0.722    110
         56.03   0.141     54
         54.93   0.138     79
         52.61   0.132    616
         49.07   0.123     54
         48.34   0.121     65
    

in CDCl3



liquid film