-
MassMS-IW-7606 dichlorodecylmethylsilane C11H24Cl2Si (Mass of molecular ion: 254)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 5.5 28.0 1.0 29.0 12.2 36.0 1.6 39.0 4.4 41.0 23.9 42.0 7.7 43.0 57.7 44.0 2.0 53.0 1.4 54.0 2.5 55.0 15.6 56.0 15.2 57.0 67.3 58.0 2.9 63.0 3.9 65.0 1.5 67.0 1.7 68.0 2.1 69.0 12.7 70.0 16.1 71.0 50.6 72.0 2.8 78.0 1.7 79.0 4.6 81.0 1.7 82.0 3.4 83.0 9.7 84.0 10.3 85.0 20.8 86.0 1.4 93.0 1.4 96.0 1.7 97.0 8.3 98.0 6.1 99.0 2.9 101.0 1.0 105.0 1.6 107.0 1.0 111.0 5.8 112.0 7.2 113.0 100.0 114.0 7.4 115.0 69.6 116.0 4.3 117.0 13.2 119.0 3.2 121.0 1.2 127.0 1.1 133.0 2.1 140.0 14.9 141.0 65.3 142.0 5.7 143.0 43.8 144.0 3.6 145.0 8.1 147.0 9.2 148.0 1.3 149.0 3.2 154.0 2.5 155.0 17.9 156.0 3.5 157.0 12.1 158.0 1.5 159.0 2.3 161.0 4.6 163.0 1.7 167.0 1.2 169.0 9.5 170.0 1.3 171.0 6.0 173.0 1.1 183.0 4.1 185.0 2.7 197.0 2.8 199.0 1.8 211.0 1.6 213.0 1.1 218.0 2.8 219.0 1.2 220.0 1.1 225.0 1.1 239.0 9.8 240.0 1.6 241.0 6.7 242.0 1.1 243.0 1.3 254.0 8.6 255.0 1.5 256.0 5.8 257.0 1.0 258.0 1.1
400 MHz in CDCl3
-
1H NMR 399.65 MHz C11 H24 Cl2 Si 0.05 ml : 0.5 ml CDCl3 dichlorodecylmethylsilane 
Assign. Shift(ppm)
A 1.50 B 1.37 C 1.27 D 1.107 E 0.882 F 0.758
Hz ppm Int.607.91 1.522 39 605.96 1.517 30 600.34 1.503 66 599.12 1.500 58 596.44 1.493 34 594.73 1.489 43 592.29 1.483 73 589.36 1.475 40 584.59 1.463 32 583.62 1.461 31 554.69 1.388 42 552.61 1.383 38 547.85 1.371 58 540.89 1.354 48 540.65 1.353 48 536.62 1.343 34 533.81 1.336 41 521.12 1.304 108 507.45 1.270 638 450.93 1.129 154 445.56 1.115 60 442.38 1.107 90 434.57 1.088 127 359.62 0.900 118 352.91 0.884 376 345.83 0.866 154 303.22 0.759 1000
in CDCl3
liquid film
更多供应商
