-
MS-NW-8598 borane-triethylamine complex C6H15N H3B (Mass of molecular ion: 115)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
13.0 1.3 15.0 1.7 18.0 1.8 26.0 1.7 27.0 11.2 28.0 10.6 29.0 15.9 30.0 26.4 39.0 1.3 40.0 2.5 41.0 3.1 42.0 10.8 43.0 1.7 44.0 11.5 53.0 1.9 54.0 7.8 55.0 1.5 56.0 7.9 57.0 1.8 58.0 28.3 59.0 1.0 68.0 1.1 69.0 1.4 70.0 8.1 71.0 1.5 72.0 4.0 81.0 1.4 82.0 5.4 83.0 3.9 84.0 14.7 85.0 1.5 86.0 100.0 87.0 6.0 98.0 1.2 100.0 12.5 101.0 17.2 102.0 1.3 113.0 3.7 114.0 15.0 115.0 1.0
400 MHz in CDCl3
-
1H NMR 399.65 MHz C6 H15 N 0.05 ml : 0.5 ml CDCl3 borane-triethylamine complex Assign. Shift(ppm)
A 2.784 B 1.6 C 1.189
Hz ppm Int.
1123.78 2.812 227 1116.46 2.794 531 1109.13 2.776 543 1101.81 2.757 237 538.45 1.348 20 482.91 1.209 697 475.46 1.190 1000 468.26 1.172 709 454.10 1.137 28 447.27 1.120 22 446.90 1.119 22 446.66 1.118 22 444.70 1.113 21
更多供应商