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硼烷二甲硫醚络合物

产品名称 硼烷二甲硫醚络合物

CAS号13292-87-0

分子式C2H10BS

分子量76.97

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  • Mass

    MS-IW-3829          
    borane-dimethyl sulfide complex
    C2H6S H3B           (Mass of molecular ion:     76)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       1.4
          24.0       1.4
          26.0       2.0
          27.0       8.2
          35.0      18.1
          44.0       4.0
          45.0      35.9
          46.0      30.3
          47.0      79.8
          48.0       3.1
          49.0       3.8
          57.0       2.7
          58.0       3.4
          59.0       3.5
          61.0      38.0
          62.0     100.0
          63.0       5.0
          64.0       4.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C2 H6 S 0.05 ml : 0.5 ml CDCl3
    borane-dimethyl sulfide complex
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.264 B 1.50 J(B-11,B)=104HZ

         Hz     ppm     Int.
    

        905.03   2.265   1000
        754.76   1.889     21
        754.39   1.888     21
        650.76   1.629     24
        650.27   1.628     24
        545.65   1.366     24
        545.29   1.365     24
        544.80   1.364     24
        544.43   1.363     24
        441.28   1.105     21
        440.67   1.103     21
    

in CDCl3



liquid film