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MS-IW-3829 borane-dimethyl sulfide complex C2H6S H3B (Mass of molecular ion: 76)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.4 24.0 1.4 26.0 2.0 27.0 8.2 35.0 18.1 44.0 4.0 45.0 35.9 46.0 30.3 47.0 79.8 48.0 3.1 49.0 3.8 57.0 2.7 58.0 3.4 59.0 3.5 61.0 38.0 62.0 100.0 63.0 5.0 64.0 4.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C2 H6 S 0.05 ml : 0.5 ml CDCl3 borane-dimethyl sulfide complex Assign. Shift(ppm)
A 2.264 B 1.50 J(B-11,B)=104HZ
Hz ppm Int.
905.03 2.265 1000 754.76 1.889 21 754.39 1.888 21 650.76 1.629 24 650.27 1.628 24 545.65 1.366 24 545.29 1.365 24 544.80 1.364 24 544.43 1.363 24 441.28 1.105 21 440.67 1.103 21
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