400 MHz in CDCl3
90 MHz in CDCl3
-
1H NMR 399.65 MHz C6 H15 N 0.034 g : 0.5 ml CDCl3 triethylamine hydrochloride 
Assign. Shift(ppm)
A 11.7 B 3.155 C 1.427 J(A,B)=4.8HZ
Hz ppm Int.1274.66 3.190 94 1269.89 3.178 102 1267.33 3.172 299 1262.57 3.160 296 1260.00 3.153 310 1255.24 3.141 295 1252.68 3.135 117 1247.91 3.123 101 577.89 1.446 567 570.56 1.428 1000 563.24 1.410 539
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1H NMR 89.56 MHz C6 H15 N 0.045 g : 0.5 ml CDCl3 triethylamine hydrochloride Assign. Shift(ppm)
A 11.6 B 3.17 C 1.43 J(A,B)=5 HZ.
Hz ppm Int.297.11 3.318 62 291.89 3.260 71 289.59 3.234 228 284.72 3.180 231 282.24 3.152 247 277.37 3.098 243 275.23 3.074 89 270.36 3.019 80 135.18 1.510 508 127.92 1.429 1000 120.57 1.347 408
in CDCl3
KBr disc
nujol mull
4880 A,200 M,powder
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