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网站主页CAS数据库列表 1485-70-7更多图谱n-苄基苯甲酰胺(1485-70-7)质谱(MS)

n-苄基苯甲酰胺

产品名称 n-苄基苯甲酰胺

CAS号1485-70-7

分子式C14H13NO

分子量211.26

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  • Mass

    MS-NW-6465          
    N-benzylbenzamide
    C14H13NO            (Mass of molecular ion:    211)
    

       Source Temperature: 170 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          17.0       1.0
          18.0       5.7
          27.0       1.2
          28.0       4.2
          39.0       2.6
          50.0       3.3
          51.0      11.1
          52.0       1.5
          63.0       1.3
          65.0       4.0
          74.0       1.2
          76.0       2.1
          77.0      41.9
          78.0       5.4
          79.0       4.5
          89.0       1.3
          91.0       9.1
         103.0       1.1
         104.0       3.8
         105.0     100.0
         106.0      29.3
         107.0       3.4
         132.0       1.0
         134.0       1.5
         181.0       1.8
         182.0       1.4
         194.0       1.0
         210.0      25.4
         211.0      81.5
         212.0      12.8
         213.0       1.2
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C14 H13 N O 0.040 g : 0.5 ml CDCl3
    N-benzylbenzamide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.778 B 7.462 C 7.378 D 7.31 E 7.31 F 7.26 G 6.78 J 4.586 J(G,J) = 5.7 HZ.

         Hz     ppm     Int.
    

       3111.57   7.786    229
       3106.45   7.773     87
       3104.49   7.769    270
       3103.03   7.765    208
       2991.94   7.487     33
       2990.72   7.484     55
       2989.50   7.481     37
       2985.47   7.471     47
       2983.40   7.466    143
       2981.45   7.461     52
       2977.29   7.450     73
       2975.95   7.447    114
       2974.73   7.444     65
       2954.96   7.394    200
       2953.61   7.391    102
       2948.49   7.378    173
       2947.27   7.375    287
       2941.53   7.361     64
       2940.06   7.357    125
       2935.30   7.345     31
       2933.84   7.342     35
       2932.74   7.339     41
       2931.27   7.335     47
       2924.44   7.318    411
       2920.41   7.308   1000
       2916.26   7.298     76
       2914.55   7.293     67
       2910.40   7.283    104
       2907.35   7.275     87
       2905.88   7.272     91
       2901.73   7.261     87
       2899.41   7.255     40
       2896.85   7.249     50
       2894.90   7.244    114
       2707.89   6.776     42
       1835.21   4.593    373
       1829.47   4.578    365
    


  • 1H NMR 89.56 MHz
    C14 H13 N O 0.047 g : 0.5 ml CDCl3
    N-benzylbenzamide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.78 B 7.49 to 7.38 C 7.38 to 7.30 D 6.5 E 4.628 J(D,E)=5.7HZ 400MHZ : HSP-41-749

         Hz     ppm     Int.
    

        702.48   7.844     84
        700.60   7.823     96
        698.80   7.803     39
        698.38   7.798     42
        697.44   7.788     61
        695.56   7.767     88
        692.74   7.735    152
        672.06   7.505     41
        671.46   7.498     53
        668.55   7.465    219
        667.10   7.449    194
        666.16   7.439    121
        664.28   7.418     69
        663.00   7.403     81
        661.98   7.392     82
        661.21   7.383    110
        656.51   7.331   1000
        652.66   7.288     52
        417.33   4.660    226
        411.61   4.596    211
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder