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MS-IW-4067 (R)-(+)-1-(p-tolyl)ethylamine C9H13N (Mass of molecular ion: 135)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 5.6 39.0 2.6 41.0 1.5 42.0 9.1 43.0 5.4 44.0 9.5 51.0 2.0 58.5 1.4 59.5 5.6 60.0 3.1 63.0 1.6 65.0 5.0 66.5 1.7 77.0 9.2 78.0 1.7 79.0 1.1 89.0 1.6 91.0 17.5 92.0 3.2 93.0 25.7 94.0 2.0 103.0 1.1 115.0 2.1 117.0 3.6 118.0 5.6 119.0 5.9 120.0 100.0 121.0 9.2 134.0 6.0 135.0 2.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H13 N 0.05 ml : 0.5 ml CDCl3 (R)-(+)-1-(p-tolyl)ethylamine Assign. Shift(ppm)
A 7.200 B 7.109 C 4.034 D 2.303 E 1.53 F 1.336
Hz ppm Int.
2882.32 7.213 322 2874.27 7.192 460 2844.36 7.118 386 2836.55 7.098 277 1622.19 4.060 54 1615.60 4.043 157 1609.01 4.027 159 1602.42 4.010 58 920.65 2.304 1000 612.30 1.533 175 540.41 1.353 73 537.60 1.346 861 533.81 1.336 73 530.88 1.329 854
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