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MS-NW-6309 N-benzylphthalimide C15H11NO2 (Mass of molecular ion: 237)
Source Temperature: 170 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 2.9 27.0 1.8 28.0 1.3 38.0 1.8 39.0 6.7 41.0 1.2 50.0 14.6 51.0 13.0 52.0 2.7 62.0 1.2 63.0 4.1 64.0 1.7 65.0 9.0 74.0 4.2 75.0 6.6 76.0 24.2 77.0 30.9 78.0 14.2 79.0 1.6 89.0 5.0 90.0 4.5 91.0 11.6 92.0 1.0 102.0 4.2 103.0 4.0 104.0 55.9 105.0 19.2 106.0 3.4 130.0 11.6 131.0 2.7 132.0 3.9 133.0 5.7 152.0 3.0 153.0 1.7 160.0 3.7 164.0 2.5 165.0 4.1 166.0 1.6 180.0 11.6 181.0 4.1 190.0 1.2 192.0 1.1 193.0 1.2 208.0 19.7 209.0 21.6 210.0 3.3 219.0 29.1 220.0 6.3 236.0 4.7 237.0 100.0 238.0 16.9 239.0 1.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C15 H11 N O2 0.047 g : 0.5 ml CDCl3 N-benzylphthalimide Assign. Shift(ppm)
A 7.82 B 7.66 C 7.53 to 7.17 D 4.834
Hz ppm Int.
705.44 7.877 235 702.56 7.845 144 701.81 7.837 159 700.63 7.824 155 699.19 7.807 286 696.88 7.782 423 696.50 7.777 451 694.88 7.759 66 693.94 7.749 145 693.50 7.744 193 692.75 7.736 152 690.19 7.707 429 689.81 7.703 439 687.50 7.677 217 686.06 7.661 160 684.88 7.648 162 684.13 7.639 141 681.25 7.607 237 671.44 7.498 54 669.50 7.476 56 667.25 7.451 121 666.69 7.445 108 666.13 7.438 93 664.88 7.424 99 664.00 7.415 122 662.94 7.403 227 660.94 7.380 284 659.00 7.359 154 658.56 7.354 159 657.19 7.338 208 655.50 7.320 319 654.75 7.311 329 653.44 7.297 230 652.31 7.284 165 651.06 7.270 225 650.00 7.258 291 647.75 7.233 339 646.06 7.214 51 644.88 7.201 30 644.38 7.195 35 433.00 4.835 1000
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