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MassMS-NW-6465 N-benzylbenzamide C14H13NO (Mass of molecular ion: 211)
Source Temperature: 170 °C Sample Temperature: 100 °C Direct, 75 eV
17.0 1.0 18.0 5.7 27.0 1.2 28.0 4.2 39.0 2.6 50.0 3.3 51.0 11.1 52.0 1.5 63.0 1.3 65.0 4.0 74.0 1.2 76.0 2.1 77.0 41.9 78.0 5.4 79.0 4.5 89.0 1.3 91.0 9.1 103.0 1.1 104.0 3.8 105.0 100.0 106.0 29.3 107.0 3.4 132.0 1.0 134.0 1.5 181.0 1.8 182.0 1.4 194.0 1.0 210.0 25.4 211.0 81.5 212.0 12.8 213.0 1.2
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C14 H13 N O 0.040 g : 0.5 ml CDCl3 N-benzylbenzamide 
Assign. Shift(ppm)
A 7.778 B 7.462 C 7.378 D 7.31 E 7.31 F 7.26 G 6.78 J 4.586 J(G,J) = 5.7 HZ.
Hz ppm Int.3111.57 7.786 229 3106.45 7.773 87 3104.49 7.769 270 3103.03 7.765 208 2991.94 7.487 33 2990.72 7.484 55 2989.50 7.481 37 2985.47 7.471 47 2983.40 7.466 143 2981.45 7.461 52 2977.29 7.450 73 2975.95 7.447 114 2974.73 7.444 65 2954.96 7.394 200 2953.61 7.391 102 2948.49 7.378 173 2947.27 7.375 287 2941.53 7.361 64 2940.06 7.357 125 2935.30 7.345 31 2933.84 7.342 35 2932.74 7.339 41 2931.27 7.335 47 2924.44 7.318 411 2920.41 7.308 1000 2916.26 7.298 76 2914.55 7.293 67 2910.40 7.283 104 2907.35 7.275 87 2905.88 7.272 91 2901.73 7.261 87 2899.41 7.255 40 2896.85 7.249 50 2894.90 7.244 114 2707.89 6.776 42 1835.21 4.593 373 1829.47 4.578 365
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1H NMR 89.56 MHz C14 H13 N O 0.047 g : 0.5 ml CDCl3 N-benzylbenzamide Assign. Shift(ppm)
A 7.78 B 7.49 to 7.38 C 7.38 to 7.30 D 6.5 E 4.628 J(D,E)=5.7HZ 400MHZ : HSP-41-749
Hz ppm Int.702.48 7.844 84 700.60 7.823 96 698.80 7.803 39 698.38 7.798 42 697.44 7.788 61 695.56 7.767 88 692.74 7.735 152 672.06 7.505 41 671.46 7.498 53 668.55 7.465 219 667.10 7.449 194 666.16 7.439 121 664.28 7.418 69 663.00 7.403 81 661.98 7.392 82 661.21 7.383 110 656.51 7.331 1000 652.66 7.288 52 417.33 4.660 226 411.61 4.596 211
in CDCl3
KBr disc
nujol mull
4880 A,200 M,powder
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