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MassMS-NW-3280 trichloro(ethyl)silane C2H5Cl3Si (Mass of molecular ion: 162)
Source Temperature: 270 °C Sample Temperature: 180 °C Reservoir, 75 eV
26.0 2.9 27.0 10.4 28.0 11.7 29.0 22.7 49.0 1.2 53.0 1.9 63.0 20.1 64.0 1.9 65.0 7.3 98.0 19.7 99.0 8.2 100.0 13.3 101.0 5.6 102.0 2.8 103.0 1.0 125.0 2.8 126.0 64.4 127.0 10.5 128.0 45.0 129.0 6.2 130.0 8.7 131.0 1.0 133.0 100.0 134.0 5.7 135.0 99.0 136.0 5.4 137.0 34.6 138.0 1.9 139.0 4.6 162.0 8.4 164.0 8.4 166.0 2.9
parameter in CDCl3
90 MHz in CDCl3
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1H NMR 300 MHz C2 H5 Cl3 Si 0.04 ml : 0.5 ml CDCl3 trichloro(ethyl)silane 
Parameter ppm Hz
D(A) 1.391 D(B) 1.179 J(A,B) 7.82
Hz ppm Int.430.36 1.435 104 428.92 1.430 110 423.31 1.411 149 421.70 1.406 376 421.24 1.404 354 415.00 1.383 272 413.66 1.379 519 407.06 1.357 217 405.83 1.353 229 361.73 1.206 387 360.89 1.203 617 353.67 1.179 1000 346.41 1.155 233 345.55 1.152 362 344.41 1.148 199
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1H NMR 89.56 MHz C2 H5 Cl3 Si 0.04 ml : 0.5 ml CDCl3 trichloro(ethyl)silane Assign. Shift(ppm)
A 1.391 B 1.179 J(A,B) = 7.8 HZ.
Hz ppm Int.139.88 1.562 31 135.88 1.518 48 135.38 1.512 29 130.38 1.456 159 128.06 1.430 182 122.00 1.363 320 121.31 1.355 324 117.56 1.313 198 116.06 1.296 239 111.69 1.248 358 110.69 1.236 280 110.06 1.229 245 105.69 1.181 1000 102.63 1.146 93 101.75 1.137 29 99.75 1.114 104 98.13 1.096 69 97.63 1.091 99 96.63 1.079 67 93.19 1.041 51
in CDCl3
liquid film
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