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网站主页CAS数据库列表 115-21-9更多图谱乙基三氯硅烷(115-21-9)核磁图(1HNMR)

乙基三氯硅烷

产品名称 乙基三氯硅烷

CAS号115-21-9

分子式C2H5Cl3Si

分子量163.51

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  • Mass

    MS-NW-3280          
    trichloro(ethyl)silane
    C2H5Cl3Si           (Mass of molecular ion:    162)
    

       Source Temperature: 270 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          26.0       2.9
          27.0      10.4
          28.0      11.7
          29.0      22.7
          49.0       1.2
          53.0       1.9
          63.0      20.1
          64.0       1.9
          65.0       7.3
          98.0      19.7
          99.0       8.2
         100.0      13.3
         101.0       5.6
         102.0       2.8
         103.0       1.0
         125.0       2.8
         126.0      64.4
         127.0      10.5
         128.0      45.0
         129.0       6.2
         130.0       8.7
         131.0       1.0
         133.0     100.0
         134.0       5.7
         135.0      99.0
         136.0       5.4
         137.0      34.6
         138.0       1.9
         139.0       4.6
         162.0       8.4
         164.0       8.4
         166.0       2.9
    

parameter in CDCl3

90 MHz in CDCl3


  • 1H NMR 300 MHz
    C2 H5 Cl3 Si 0.04 ml : 0.5 ml CDCl3
    trichloro(ethyl)silane
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 1.391 D(B) 1.179 J(A,B) 7.82

         Hz     ppm     Int.
    

        430.36   1.435    104
        428.92   1.430    110
        423.31   1.411    149
        421.70   1.406    376
        421.24   1.404    354
        415.00   1.383    272
        413.66   1.379    519
        407.06   1.357    217
        405.83   1.353    229
        361.73   1.206    387
        360.89   1.203    617
        353.67   1.179   1000
        346.41   1.155    233
        345.55   1.152    362
        344.41   1.148    199
    


  • 1H NMR 89.56 MHz
    C2 H5 Cl3 Si 0.04 ml : 0.5 ml CDCl3
    trichloro(ethyl)silane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 1.391 B 1.179 J(A,B) = 7.8 HZ.

         Hz     ppm     Int.
    

        139.88   1.562     31
        135.88   1.518     48
        135.38   1.512     29
        130.38   1.456    159
        128.06   1.430    182
        122.00   1.363    320
        121.31   1.355    324
        117.56   1.313    198
        116.06   1.296    239
        111.69   1.248    358
        110.69   1.236    280
        110.06   1.229    245
        105.69   1.181   1000
        102.63   1.146     93
        101.75   1.137     29
         99.75   1.114    104
         98.13   1.096     69
         97.63   1.091     99
         96.63   1.079     67
         93.19   1.041     51
    

in CDCl3



liquid film