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MS-NW-0096 ethylene glycol monoethyl ether C4H10O2 (Mass of molecular ion: 90)
Source Temperature: 240 °C Sample Temperature: 95 °C Reservoir, 75 eV
15.0 3.7 17.0 1.5 18.0 7.5 19.0 2.2 26.0 2.2 27.0 16.5 28.0 4.4 29.0 31.1 30.0 1.3 31.0 100.0 32.0 2.4 33.0 1.1 41.0 4.9 42.0 2.0 43.0 17.2 44.0 4.0 45.0 35.1 46.0 1.3 59.0 92.3 60.0 3.4 61.0 2.9 72.0 28.1 73.0 1.7 75.0 1.0 90.0 1.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C4 H10 O2 0.04 ml : 0.5 ml CDCl3 ethylene glycol monoethyl ether Assign. Shift(ppm)
A 3.72 B 3.55 C 3.55 D 2.70 E 1.224
Hz ppm Int.
339.44 3.791 83 338.13 3.776 101 336.38 3.756 45 335.63 3.748 103 334.69 3.738 140 334.00 3.730 157 332.75 3.716 157 331.00 3.696 85 330.06 3.686 250 329.25 3.677 280 328.56 3.669 167 321.31 3.588 734 320.56 3.580 353 319.69 3.570 131 317.88 3.550 173 316.63 3.536 165 316.00 3.529 171 314.25 3.509 579 312.56 3.490 146 311.19 3.475 115 307.31 3.432 151 242.00 2.703 768 116.44 1.301 489 109.50 1.223 1000 102.44 1.144 420
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