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网站主页CAS数据库列表 101-16-6更多图谱3-甲氧基二苯胺(101-16-6)红外图谱(IR2)

3-甲氧基二苯胺

产品名称 3-甲氧基二苯胺

CAS号101-16-6

分子式C13H13NO

分子量199.25

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  • Mass

    MS-IW-6667          
    3-methoxydiphenylamine
    C13H13NO            (Mass of molecular ion:    199)
    

       Source Temperature: 130 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          39.0       1.2
          51.0       2.9
          52.0       1.1
          63.0       1.8
          64.0       1.9
          65.0       1.7
          66.0       1.0
          77.0       4.8
          78.0       1.1
          83.5       1.9
          92.0       5.5
          93.0       1.0
          99.5       3.2
         115.0       1.0
         127.0       2.0
         128.0       4.0
         129.0       4.8
         130.0       1.2
         154.0       6.4
         155.0       3.9
         156.0       4.5
         157.0       1.1
         166.0       3.1
         167.0       7.5
         168.0       7.8
         169.0       3.7
         170.0       7.5
         171.0       1.0
         183.0       6.3
         184.0       3.1
         198.0       9.5
         199.0     100.0
         200.0      14.7
         201.0       1.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H13 N O 0.040 g : 0.5 ml CDCl3
    3-methoxydiphenylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.252 B 7.148 C 7.072 D 6.928 E 6.64 F 6.62 G 6.471 J 5.69 K 3.752

         Hz     ppm     Int.
    

       2906.98   7.274    109
       2906.25   7.272     50
       2905.03   7.269     44
       2900.51   7.258     63
       2899.66   7.256    155
       2898.44   7.253    173
       2896.48   7.248     31
       2893.19   7.240     53
       2891.97   7.237     61
       2891.11   7.235    154
       2865.72   7.171     60
       2858.76   7.154     46
       2857.30   7.150    117
       2856.57   7.148     89
       2849.98   7.132     59
       2849.12   7.130     70
       2832.40   7.088     32
       2831.54   7.086     42
       2830.57   7.083    169
       2829.35   7.080    200
       2828.61   7.078    107
       2827.27   7.075     56
       2823.85   7.066     53
       2822.88   7.064     87
       2821.90   7.061    159
       2820.80   7.059    140
       2776.86   6.949     38
       2775.76   6.946     67
       2774.66   6.943     39
       2769.41   6.930     53
       2768.43   6.928    115
       2767.58   6.926     52
       2762.21   6.912     33
       2761.11   6.909     56
       2760.01   6.907     30
       2656.62   6.648     52
       2655.76   6.646     61
       2654.42   6.642     85
       2653.56   6.640     88
       2649.05   6.629     83
       2647.58   6.625    239
       2646.73   6.623    145
       2646.00   6.621    208
       2644.53   6.618     62
       2591.55   6.485     64
       2590.70   6.483     68
       2589.11   6.479     61
       2588.26   6.477     60
       2583.37   6.465     60
       2581.79   6.461     83
       2580.08   6.456     53
       1499.88   3.753   1000
    

in CDCl3



KBr disc



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