-
MassMS-IW-0584 3-methyldiphenylamine C13H13N (Mass of molecular ion: 183)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 1.0 39.0 4.8 41.0 1.0 50.0 1.5 51.0 6.4 52.0 1.8 63.0 2.9 64.0 1.5 65.0 7.2 66.0 3.3 76.0 1.6 77.0 10.4 77.5 1.5 78.0 3.2 79.0 3.7 80.0 3.2 83.5 3.6 84.0 1.0 89.0 2.3 89.5 1.8 90.0 5.4 90.5 9.1 91.0 6.8 91.5 1.3 92.0 1.1 104.0 1.3 106.0 1.1 115.0 2.2 128.0 1.6 139.0 1.3 140.0 1.2 141.0 2.1 152.0 1.4 153.0 1.1 154.0 1.4 155.0 1.2 156.0 1.2 166.0 3.1 167.0 32.0 168.0 14.8 169.0 3.5 180.0 5.9 181.0 4.1 182.0 26.1 183.0 100.0 184.0 14.4
400 MHz in CDCl3
-
1H NMR 399.65 MHz C13 H13 N 0.05 ml : 0.5 ml CDCl3 3-methyldiphenylamine 
Assign. Shift(ppm)
A 7.201 B 7.099 C 6.988 D 6.873 E 6.82 F 6.81 G 6.709 J 5.5 K 2.248
Hz ppm Int.2886.72 7.224 189 2884.64 7.218 71 2881.47 7.210 41 2879.27 7.205 277 2878.05 7.202 310 2876.10 7.197 58 2872.68 7.188 91 2870.73 7.184 282 2868.65 7.178 45 2845.70 7.121 76 2844.48 7.118 51 2838.26 7.102 133 2837.16 7.100 150 2830.81 7.084 81 2829.71 7.081 98 2799.44 7.005 52 2797.61 7.001 271 2796.39 6.998 342 2794.43 6.993 102 2790.89 6.984 92 2789.92 6.981 156 2788.94 6.979 291 2787.84 6.976 253 2785.64 6.971 40 2754.76 6.893 68 2753.66 6.891 113 2752.56 6.888 63 2747.56 6.875 101 2746.34 6.872 197 2745.48 6.870 102 2740.11 6.857 59 2739.01 6.854 96 2737.92 6.851 52 2730.35 6.832 76 2728.52 6.828 119 2721.31 6.810 349 2720.70 6.808 344 2684.69 6.718 125 2684.08 6.717 112 2677.61 6.700 118 2677.00 6.699 117 898.56 2.249 1000
in CDCl3
liquid film
更多供应商
