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网站主页CAS数据库列表 1205-64-7更多图谱3-甲基二苯胺(1205-64-7)质谱(MS)

3-甲基二苯胺

产品名称 3-甲基二苯胺

CAS号1205-64-7

分子式C13H13N

分子量183.25

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  • Mass

    MS-IW-0584          
    3-methyldiphenylamine
    C13H13N             (Mass of molecular ion:    183)
    

       Source Temperature: 260 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       1.0
          39.0       4.8
          41.0       1.0
          50.0       1.5
          51.0       6.4
          52.0       1.8
          63.0       2.9
          64.0       1.5
          65.0       7.2
          66.0       3.3
          76.0       1.6
          77.0      10.4
          77.5       1.5
          78.0       3.2
          79.0       3.7
          80.0       3.2
          83.5       3.6
          84.0       1.0
          89.0       2.3
          89.5       1.8
          90.0       5.4
          90.5       9.1
          91.0       6.8
          91.5       1.3
          92.0       1.1
         104.0       1.3
         106.0       1.1
         115.0       2.2
         128.0       1.6
         139.0       1.3
         140.0       1.2
         141.0       2.1
         152.0       1.4
         153.0       1.1
         154.0       1.4
         155.0       1.2
         156.0       1.2
         166.0       3.1
         167.0      32.0
         168.0      14.8
         169.0       3.5
         180.0       5.9
         181.0       4.1
         182.0      26.1
         183.0     100.0
         184.0      14.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H13 N 0.05 ml : 0.5 ml CDCl3
    3-methyldiphenylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.201 B 7.099 C 6.988 D 6.873 E 6.82 F 6.81 G 6.709 J 5.5 K 2.248

         Hz     ppm     Int.
    

       2886.72   7.224    189
       2884.64   7.218     71
       2881.47   7.210     41
       2879.27   7.205    277
       2878.05   7.202    310
       2876.10   7.197     58
       2872.68   7.188     91
       2870.73   7.184    282
       2868.65   7.178     45
       2845.70   7.121     76
       2844.48   7.118     51
       2838.26   7.102    133
       2837.16   7.100    150
       2830.81   7.084     81
       2829.71   7.081     98
       2799.44   7.005     52
       2797.61   7.001    271
       2796.39   6.998    342
       2794.43   6.993    102
       2790.89   6.984     92
       2789.92   6.981    156
       2788.94   6.979    291
       2787.84   6.976    253
       2785.64   6.971     40
       2754.76   6.893     68
       2753.66   6.891    113
       2752.56   6.888     63
       2747.56   6.875    101
       2746.34   6.872    197
       2745.48   6.870    102
       2740.11   6.857     59
       2739.01   6.854     96
       2737.92   6.851     52
       2730.35   6.832     76
       2728.52   6.828    119
       2721.31   6.810    349
       2720.70   6.808    344
       2684.69   6.718    125
       2684.08   6.717    112
       2677.61   6.700    118
       2677.00   6.699    117
        898.56   2.249   1000
    

in CDCl3



liquid film