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网站主页CAS数据库列表 101-54-2更多图谱对氨基二苯胺(101-54-2)核磁图(1HNMR)

对氨基二苯胺

产品名称 对氨基二苯胺

CAS号101-54-2

分子式C12H12N2

分子量184.24

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  • Mass

    MS-NW-0736          
    N-phenyl-p-phenylenediamine
    C12H12N2            (Mass of molecular ion:    184)
    

       Source Temperature: 140 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          28.0       1.1
          39.0       2.3
          51.0       2.8
          52.0       1.9
          53.0       2.0
          63.0       1.3
          65.0       3.4
          66.0       1.2
          77.0       3.5
          78.0       1.5
          79.0       1.3
          80.0       5.6
          81.0       2.1
          83.5       1.7
          91.0       5.7
          91.5       1.9
          92.0       5.5
          93.0       1.6
         106.0       1.0
         107.0      15.0
         108.0       1.1
         118.0       2.4
         128.0       1.4
         129.0       1.0
         130.0       1.3
         154.0       1.5
         156.0       1.8
         166.0       4.4
         167.0       4.1
         168.0       1.5
         181.0       2.1
         182.0       4.6
         183.0      12.7
         184.0     100.0
         185.0      13.8
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H12 N2 0.038 g : 0.5 ml CDCl3
    N-phenyl-p-phenylenediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.172 B 6.948 C 6.831 D 6.777 E 6.633 F 5.39 G 3.51

         Hz     ppm     Int.
    

       2876.59   7.198     64
       2874.51   7.193    411
       2873.66   7.191    180
       2872.44   7.188    154
       2869.51   7.181     84
       2867.92   7.177    212
       2867.19   7.175    544
       2865.84   7.171    558
       2863.77   7.166     97
       2860.60   7.158    173
       2859.50   7.156    191
       2858.52   7.153    501
       2856.45   7.148     73
       2784.55   6.968     93
       2781.37   6.960    835
       2779.05   6.954    279
       2777.10   6.949     48
       2776.86   6.949     48
       2774.90   6.944    297
       2772.58   6.938    960
       2769.53   6.930    103
       2736.57   6.848     91
       2735.72   6.846    117
       2734.50   6.843    508
       2733.40   6.840    679
       2732.54   6.838    345
       2731.32   6.835    195
       2727.91   6.826    165
       2726.81   6.823    290
       2725.83   6.821    555
       2724.85   6.819    512
       2722.53   6.813     70
       2716.80   6.798    146
       2715.70   6.796    233
       2714.60   6.793    131
       2709.35   6.780    187
       2708.37   6.777    395
       2707.52   6.775    175
       2702.15   6.762    114
       2701.05   6.759    199
       2699.95   6.756    109
       2658.20   6.652    122
       2655.15   6.644   1000
       2652.83   6.638    324
       2650.88   6.634     48
       2648.56   6.628    294
       2646.36   6.622    850
       2643.19   6.614     92
       2155.64   5.394     71
       2155.15   5.393     72
       1402.83   3.511    123
       1402.34   3.509    123
    

in CDCl3



CCl4 solution



KBr disc



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