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MassMS-NW-0736 N-phenyl-p-phenylenediamine C12H12N2 (Mass of molecular ion: 184)
Source Temperature: 140 °C Sample Temperature: 120 °C Direct, 75 eV
28.0 1.1 39.0 2.3 51.0 2.8 52.0 1.9 53.0 2.0 63.0 1.3 65.0 3.4 66.0 1.2 77.0 3.5 78.0 1.5 79.0 1.3 80.0 5.6 81.0 2.1 83.5 1.7 91.0 5.7 91.5 1.9 92.0 5.5 93.0 1.6 106.0 1.0 107.0 15.0 108.0 1.1 118.0 2.4 128.0 1.4 129.0 1.0 130.0 1.3 154.0 1.5 156.0 1.8 166.0 4.4 167.0 4.1 168.0 1.5 181.0 2.1 182.0 4.6 183.0 12.7 184.0 100.0 185.0 13.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H12 N2 0.038 g : 0.5 ml CDCl3 N-phenyl-p-phenylenediamine 
Assign. Shift(ppm)
A 7.172 B 6.948 C 6.831 D 6.777 E 6.633 F 5.39 G 3.51
Hz ppm Int.2876.59 7.198 64 2874.51 7.193 411 2873.66 7.191 180 2872.44 7.188 154 2869.51 7.181 84 2867.92 7.177 212 2867.19 7.175 544 2865.84 7.171 558 2863.77 7.166 97 2860.60 7.158 173 2859.50 7.156 191 2858.52 7.153 501 2856.45 7.148 73 2784.55 6.968 93 2781.37 6.960 835 2779.05 6.954 279 2777.10 6.949 48 2776.86 6.949 48 2774.90 6.944 297 2772.58 6.938 960 2769.53 6.930 103 2736.57 6.848 91 2735.72 6.846 117 2734.50 6.843 508 2733.40 6.840 679 2732.54 6.838 345 2731.32 6.835 195 2727.91 6.826 165 2726.81 6.823 290 2725.83 6.821 555 2724.85 6.819 512 2722.53 6.813 70 2716.80 6.798 146 2715.70 6.796 233 2714.60 6.793 131 2709.35 6.780 187 2708.37 6.777 395 2707.52 6.775 175 2702.15 6.762 114 2701.05 6.759 199 2699.95 6.756 109 2658.20 6.652 122 2655.15 6.644 1000 2652.83 6.638 324 2650.88 6.634 48 2648.56 6.628 294 2646.36 6.622 850 2643.19 6.614 92 2155.64 5.394 71 2155.15 5.393 72 1402.83 3.511 123 1402.34 3.509 123
in CDCl3
CCl4 solution
KBr disc
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