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MassMS-NW-3599 2,4-toluenediamine C7H10N2 (Mass of molecular ion: 122)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
18.0 2.2 27.0 2.3 28.0 4.7 30.0 1.2 38.0 1.3 39.0 4.1 40.0 2.1 41.0 4.6 42.0 3.8 50.0 2.1 51.0 4.9 52.0 4.7 53.0 3.7 54.0 3.3 60.0 1.4 60.5 1.4 61.0 4.5 63.0 1.1 65.0 3.4 66.0 3.3 67.0 4.0 68.0 1.0 76.0 1.1 77.0 10.9 78.0 6.1 79.0 1.8 80.0 4.0 81.0 1.8 92.0 1.6 93.0 5.5 94.0 18.4 95.0 3.0 104.0 11.1 105.0 13.9 106.0 7.7 119.0 1.6 121.0 96.2 122.0 100.0 123.0 8.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H10 N2 0.047 g : 0.5 ml CDCl3 2,4-toluenediamine 
Assign. Shift(ppm)
A 6.79 B 6.03 C 5.99 D 3.45 E 2.03
Hz ppm Int.612.81 6.843 101 612.13 6.835 143 611.38 6.827 99 605.31 6.759 116 604.63 6.752 180 603.88 6.743 132 602.38 6.726 24 546.75 6.105 110 544.44 6.080 174 539.00 6.019 31 536.69 5.993 416 534.81 5.972 117 534.50 5.969 117 308.50 3.445 709 182.38 2.037 926 182.00 2.033 1000
in CDCl3
KBr disc
nujol mull
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