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m-Xylene

Product Name m-Xylene

CAS108-38-3

MFC8H10

MW106.17

¹³CNMR

Mass

MS-NW-0045          
m-xylene
C8H10               (Mass of molecular ion:    106)

   Source Temperature: 222 °C
   Sample Temperature:  55 °C
   Reservoir, 75 eV

      27.0       2.7
      28.0       1.3
      38.0       1.2
      39.0       7.7
      41.0       1.2
      50.0       2.7
      51.0       7.5
      52.0       3.4
      53.0       2.1
      62.0       1.6
      63.0       4.7
      65.0       6.0
      74.0       1.1
      77.0      11.3
      78.0       5.6
      79.0       7.1
      89.0       1.9
      91.0     100.0
      92.0       7.6
     102.0       1.1
     103.0       6.0
     104.0       2.6
     105.0      28.8
     106.0      71.0
     107.0       6.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₁₀	0.05 ml : 0.5 ml CDCl₃
m-xylene

    Assign.     Shift(ppm)

      A             7.109
      B             6.96
      C             6.94
      D             2.278

     Hz     ppm     Int.

   2849.49   7.130     58
   2841.80   7.111    125
   2834.47   7.093     81
   2783.33   6.965     52
   2781.25   6.960    122
   2780.64   6.958    141
   2779.91   6.956    146
   2779.17   6.955    146
   2778.44   6.953    165
   2777.83   6.951    192
   2777.22   6.950    203
   2776.61   6.948    187
   2769.90   6.931    140
   2769.41   6.930    147
   2768.68   6.928    139
   2768.07   6.927    120
    910.64   2.279   1000
    910.28   2.278    994

in CDCl3

liquid film

4880 A,200 M,liquid

ANION RADICAL, REDUCTION WITH NA OR K IN DME

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