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Methanol

Product Name Methanol

CAS67-56-1

MFCH4O

MW32.04

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  • Mass 

    MS-NW-0072          
methanol
CH4O                (Mass of molecular ion:     32)


       Source Temperature: 220 °C
   Sample Temperature:  25 °C
   Reservoir, 75 eV


          14.0       1.7
      15.0      12.4
      28.0       4.6
      29.0      44.6
      30.0       6.5
      31.0     100.0
      32.0      74.4
      33.0       1.2

in CD3CN

90 MHz in CDCl3

in DMSO-d6

in CDCl3

parameter in CDCl3




  • 1H NMR 89.56 MHz
    C H4 O 0.05 ml : 0.5 ml CDCl3
    methanol
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             3.66
      B             3.43
     
     J(A,B)=4.6HZ.
  

         Hz     ppm     Int.


        336.81   3.761     36
    331.25   3.699    135
    326.13   3.642    188
    321.75   3.593    124
    308.63   3.447   1000
    304.00   3.395    562






  • 1H NMR 300 MHz
    C H4 O 0.1 ml : 0.5 ml CDCl3
    methanol
    ChemicalStructure 
        Parameter     ppm  Hz
    
      D(A)         4.19
     
      D(B)         3.410
  

         Hz     ppm     Int.


       1257.00   4.190    208
   1023.00   3.410   1000

in DMSO-d6

in CD3CN

in CDCl3

in CD3OD









liquid film



4880 A,200 M,liquid



REDUCTION WITH TICL3 AND H2O2



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