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MS-KW-0100 dichloroethylsilane C2H6Cl2Si (Mass of molecular ion: 128)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 1.9 27.0 7.5 28.0 5.6 29.0 11.6 36.0 2.8 53.0 2.9 63.0 30.9 64.0 7.0 65.0 16.7 66.0 2.7 67.0 2.3 91.0 1.9 92.0 17.9 93.0 7.5 94.0 6.4 95.0 2.7 98.0 60.9 99.0 100.0 100.0 46.3 101.0 67.3 102.0 10.9 103.0 12.4 113.0 1.2 115.0 1.3 125.0 1.0 126.0 1.5 127.0 67.9 128.0 21.2 129.0 47.5 130.0 13.8 131.0 10.1 132.0 2.5 133.0 1.5 135.0 1.0 143.0 1.0 145.0 1.4 173.0 1.5 175.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C2 H6 Cl2 Si 0.05 ml : 0.5 ml CDCl3 dichloroethylsilane Assign. Shift(ppm)
A 5.497 B 1.19 C 1.13
Hz ppm Int.
2198.36 5.501 265 2196.90 5.498 490 2195.31 5.494 293 490.36 1.227 45 488.89 1.224 44 486.94 1.219 61 485.23 1.215 102 483.89 1.211 63 483.15 1.209 45 480.96 1.204 195 479.37 1.200 301 477.54 1.195 197 473.63 1.186 157 472.66 1.183 342 472.05 1.182 378 471.07 1.179 333 470.46 1.178 298 467.65 1.171 210 466.19 1.167 336 464.60 1.163 260 462.40 1.158 68 458.25 1.147 546 457.15 1.144 558 451.54 1.130 1000 448.97 1.124 179 445.19 1.114 255 443.36 1.110 202 442.63 1.108 140 439.70 1.101 100
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