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Ethyltrichlorosilane

Product Name Ethyltrichlorosilane

CAS115-21-9

MFC2H5Cl3Si

MW163.51

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¹HNMR

¹³CNMR

IR1

Mass

MS-NW-3280          
trichloro(ethyl)silane
C2H5Cl3Si           (Mass of molecular ion:    162)

   Source Temperature: 270 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      26.0       2.9
      27.0      10.4
      28.0      11.7
      29.0      22.7
      49.0       1.2
      53.0       1.9
      63.0      20.1
      64.0       1.9
      65.0       7.3
      98.0      19.7
      99.0       8.2
     100.0      13.3
     101.0       5.6
     102.0       2.8
     103.0       1.0
     125.0       2.8
     126.0      64.4
     127.0      10.5
     128.0      45.0
     129.0       6.2
     130.0       8.7
     131.0       1.0
     133.0     100.0
     134.0       5.7
     135.0      99.0
     136.0       5.4
     137.0      34.6
     138.0       1.9
     139.0       4.6
     162.0       8.4
     164.0       8.4
     166.0       2.9

parameter in CDCl3

90 MHz in CDCl3

¹H NMR	300 MHz
C₂ H₅ Cl₃ Si	0.04 ml : 0.5 ml CDCl₃
trichloro(ethyl)silane

    Parameter     ppm  Hz

      D(A)         1.391
      D(B)         1.179
       J(A,B)          7.82

     Hz     ppm     Int.

    430.36   1.435    104
    428.92   1.430    110
    423.31   1.411    149
    421.70   1.406    376
    421.24   1.404    354
    415.00   1.383    272
    413.66   1.379    519
    407.06   1.357    217
    405.83   1.353    229
    361.73   1.206    387
    360.89   1.203    617
    353.67   1.179   1000
    346.41   1.155    233
    345.55   1.152    362
    344.41   1.148    199

¹H NMR	89.56 MHz
C₂ H₅ Cl₃ Si	0.04 ml : 0.5 ml CDCl₃
trichloro(ethyl)silane

    Assign.     Shift(ppm)

      A             1.391
      B             1.179
     
     J(A,B) = 7.8 HZ.

     Hz     ppm     Int.

    139.88   1.562     31
    135.88   1.518     48
    135.38   1.512     29
    130.38   1.456    159
    128.06   1.430    182
    122.00   1.363    320
    121.31   1.355    324
    117.56   1.313    198
    116.06   1.296    239
    111.69   1.248    358
    110.69   1.236    280
    110.06   1.229    245
    105.69   1.181   1000
    102.63   1.146     93
    101.75   1.137     29
     99.75   1.114    104
     98.13   1.096     69
     97.63   1.091     99
     96.63   1.079     67
     93.19   1.041     51

in CDCl3

liquid film

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