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MassMS-NW-4921 dichloro(methyl)silane CH4Cl2Si (Mass of molecular ion: 114)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.7 28.0 2.3 29.0 1.4 35.0 1.2 36.0 2.7 41.0 3.0 42.0 4.1 43.0 5.9 63.0 29.2 64.0 2.5 65.0 10.7 77.0 2.2 78.0 11.3 79.0 18.9 80.0 5.0 81.0 6.8 98.0 9.5 99.0 38.4 100.0 8.2 101.0 26.6 102.0 2.5 103.0 4.9 112.0 1.0 113.0 100.0 114.0 8.4 115.0 65.5 116.0 5.1 117.0 12.2 118.0 1.0
parameter in CDCl3
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1H NMR 300 MHz C H4 Cl2 Si 0.04 ml : 0.5 ml CDCl3 dichloro(methyl)silane 
Parameter ppm Hz
D(A) 5.586 D(B) 0.879 J(A,B) 2.3 J(A,Si-29)= 224 Hz. J(B,Si-29)= 8 Hz.
Hz ppm Int.1679.25 5.597 89 1676.94 5.590 252 1674.71 5.582 253 1672.39 5.575 90 264.86 0.883 1000 262.59 0.875 997
in CDCl3
liquid film
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