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MS-NW-7689 triethylsilane C6H16Si (Mass of molecular ion: 116)
Source Temperature: 260 °C Sample Temperature: 170 °C Reservoir, 75 eV
27.0 2.2 28.0 1.0 29.0 4.9 31.0 10.1 43.0 7.3 44.0 1.3 45.0 3.5 53.0 1.6 55.0 3.4 56.0 2.1 57.0 6.3 58.0 10.5 59.0 100.0 60.0 7.6 61.0 3.7 73.0 1.0 86.0 22.0 87.0 87.5 88.0 8.8 89.0 3.3 115.0 2.6 116.0 3.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H16 Si 0.05 ml : 0.5 ml CDCl3 triethylsilane Assign. Shift(ppm)
A 3.621 B 0.980 C 0.591 J(A,C)=3.1HZ J(A,SI-29)=-177HZ
Hz ppm Int.
1453.49 3.637 43 1450.32 3.629 97 1447.14 3.622 126 1444.09 3.614 98 1440.92 3.606 43 411.74 1.031 36 403.81 1.011 83 399.41 1.000 509 395.02 0.989 107 391.24 0.979 1000 388.06 0.971 101 383.54 0.960 649 379.39 0.950 68 248.66 0.623 139 245.61 0.615 151 241.09 0.604 343 237.92 0.596 347 233.15 0.584 330 229.98 0.576 330 225.34 0.564 108 224.85 0.563 112 221.80 0.555 105
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