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Dibenzyl phosphate

Product Name Dibenzyl phosphate

CAS1623-08-1

MFC14H15O4P

MW278.24

¹³CNMR

Mass

MS-IW-4007          
dibenzyl hydrogen phosphate
C14H15O4P           (Mass of molecular ion:    278)

   Source Temperature: 180 °C
   Sample Temperature: 150 °C
   Direct, 75 eV

      39.0       1.6
      51.0       1.3
      63.0       1.3
      65.0       8.1
      77.0       3.2
      79.0       3.7
      89.0       2.6
      90.0       2.5
      91.0     100.0
      92.0      10.6
     105.0       2.9
     107.0      12.0
     108.0       1.7
     178.0       1.1
     179.0       3.8
     180.0       8.6
     181.0       1.4
     187.0      14.7
     188.0       1.6
     277.0      20.2
     278.0       3.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₁₅ O₄ P	0.05 ml : 0.5 ml CDCl₃
dibenzyl hydrogen phosphate

    Assign.     Shift(ppm)

      A            11.78
      B          7.32 to 7.28
      C             5.003
     
     J(C,P-31)=7.5HZ

     Hz     ppm     Int.

   4708.86  11.783     64
   2924.65   7.319     57
   2923.28   7.315     57
   2920.84   7.309    232
   2918.70   7.304   1000
   2915.95   7.297    271
   2913.82   7.291     91
   2911.53   7.286     48
   2909.85   7.281     39
   2909.24   7.280     39
   2908.17   7.277     36
   2000.89   5.007    270
   1993.41   4.988    270

in CDCl3

KBr disc

nujol mull

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