-
MS-NW-0783 triethyl phosphate C6H15O4P (Mass of molecular ion: 182)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 3.0 18.0 1.5 19.0 1.3 26.0 3.9 27.0 19.3 28.0 12.3 29.0 29.9 31.0 6.5 32.0 1.0 42.0 1.1 43.0 8.6 44.0 3.0 45.0 22.1 47.0 3.4 63.0 1.1 65.0 6.8 81.0 49.3 82.0 35.2 83.0 12.1 91.0 11.0 93.0 1.9 99.0 100.0 109.0 44.7 110.0 9.6 111.0 13.7 125.0 19.0 126.0 6.7 127.0 57.5 128.0 1.5 137.0 11.9 138.0 10.9 139.0 9.7 153.0 4.9 154.0 1.7 155.0 93.5 156.0 4.3 167.0 4.3 181.0 2.9 182.0 12.7 183.0 1.4
parameter in CDCl3
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1H NMR 300 MHz C6 H15 O4 P 0.05 ml : 0.5 ml CDCl3 triethyl phosphate Parameter ppm Hz
D(A) 4.111 D(B) 1.349 J(A,B) 7.1 J(A,P-31) 8.0 J(B,P-31) 0.9
Hz ppm Int.
1247.99 4.160 140 1240.91 4.136 447 1240.04 4.133 210 1233.78 4.113 496 1232.90 4.110 495 1226.62 4.089 216 1225.80 4.086 452 1218.72 4.062 147 412.21 1.374 506 411.36 1.371 504 405.11 1.350 1000 404.28 1.348 982 398.00 1.327 495 397.20 1.324 493
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