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2,2,4,4,6,6-Hexamethylcyclotrisilazane

Product Name 2,2,4,4,6,6-Hexamethylcyclotrisilazane

CAS1009-93-4

MFC6H21N3Si3

MW219.51

¹³CNMR

Mass

MS-IW-9303          
2,2,4,4,6,6-hexamethylcyclotrisilazane
C6H21N3Si3          (Mass of molecular ion:    219)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      73.0       1.8
      74.0       1.4
      86.0       2.2
      86.5       4.4
      87.0       1.5
      94.5      14.9
      95.0       3.3
      95.5       1.7
     100.0       2.3
     101.0       2.1
     102.0       1.1
     114.0       1.9
     115.0       1.2
     116.0       1.5
     117.0       1.3
     128.0       1.2
     130.0       2.1
     131.0       3.2
     158.0       1.3
     171.0       4.7
     172.0       1.8
     173.0       1.8
     187.0       7.3
     188.0       9.1
     189.0       3.7
     190.0       1.6
     204.0     100.0
     205.0      23.5
     206.0      12.6
     207.0       2.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₂₁ N₃ Si₃	0.05 ml : 0.5 ml CDCl₃
2,2,4,4,6,6-hexamethylcyclotrisilazane

    Assign.     Shift(ppm)

      A             0.55
      B             0.098

     Hz     ppm     Int.

     53.83   0.135     99
     39.43   0.099    956
     38.82   0.098   1000
     28.69   0.072     93

in CDCl3

liquid film

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