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D-Glucurone

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D-Glucurone Basic information
D-Glucurone Chemical Properties
  • Melting point:172-175 °C(lit.)
  • alpha 19 º (c=10, H2O)
  • Boiling point:227.71°C (rough estimate)
  • Density 1,76 g/cm3
  • refractive index 18.5 ° (C=5, H2O)
  • storage temp. Store at RT.
  • solubility water: soluble25mg/mL, clear, colorless
  • form Crystals or Crystalline Powder
  • pka11.96±0.60(Predicted)
  • color White
  • optical activity[α]24/D +18.8°, c = 8 in H2O
  • Water Solubility SOLUBLE
  • Merck 14,4467
  • BRN 83595
  • InChIKeyOGLCQHRZUSEXNB-IEPORWDDSA-N
  • CAS DataBase Reference32449-92-6(CAS DataBase Reference)
  • EPA Substance Registry SystemD-Glucuronolactone (32449-92-6)
Safety Information
  • Hazard Codes Xi
  • Risk Statements 36/37/38
  • Safety Statements 24/25-36-26
  • WGK Germany 2
  • RTECS LZ8930000
  • TSCA Yes
  • HS Code 29322980
MSDS
D-Glucurone Usage And Synthesis
  • Chemical Propertieswhite crystals or crystalline powder
  • UsesD-Glucurone is a glucuronic acid derivative. It is used for treating canine hepatitis.
  • DefinitionThe γ-lactone of glucuronic acid. Found in plant gums and animal connective tissues.
  • Purification MethodsDissolve the lactone or mixture of lactone and acid in H2O and concentrate on a steam bath until crystallisation begins. Cool rapidly to room temperature wih stirring. After 2hours the product is filtered off, washed with cold EtOH and dried to m 174-175o and [] D +19.8o (c 5.2, H2O). The amount of free acid can be obtained by titration of an ice-cold aqueous solution with standard alkali. It can be recrystallised from EtOH, EtOH/H2O or MeOH, and the highest recorded m is 180o. [Stacey J Chem Soc 1529 1939, Mehltretter et al. J Am Chem Soc 73 2424 1951, Beilstein 18 III/IV 3055, 18/5 V 33.]
D-Glucurone Preparation Products And Raw materials
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