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4-Iodophenol

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4-Iodophenol Basic information
4-Iodophenol Chemical Properties
  • Melting point:92-94 °C(lit.)
  • Boiling point:138 °C5 mm Hg(lit.)
  • Density 1.8573
  • Flash point:138°C/5mm
  • pka9.33(at 25℃)
  • form Crystals or Crystalline Powder
  • color Pink or beige to brown
  • Water Solubility slightly soluble
  • Sensitive Light Sensitive
  • Merck 14,5036
  • BRN 1904544
  • Stability:Stable. Incompatible with strong oxidizing agents.
  • CAS DataBase Reference540-38-5(CAS DataBase Reference)
  • NIST Chemistry ReferencePhenol, 4-iodo-(540-38-5)
  • EPA Substance Registry Systemp-Iodophenol (540-38-5)
Safety Information
MSDS
4-Iodophenol Usage And Synthesis
  • Chemical Propertieslight brown powder
  • Usessuzuki reaction
  • Uses4-Iodophenol is used in chemiluminescence imaging assays and experiments, as diagnostic agents in order to detect cancer cells in patients. Also it is used in the synthesis of agonists towards the est rogen β receptor.
  • Synthesis Reference(s)Organic Syntheses, Coll. Vol. 2, p. 355, 1943
    The Journal of Organic Chemistry, 70, p. 8590, 2005 DOI: 10.1021/jo051191x
    Tetrahedron Letters, 40, p. 6051, 1999 DOI: 10.1016/S0040-4039(99)01236-8
  • Purification MethodsCrystallise 4-iodophenol from pet ether (b 80-100o) or distil it in vacuo. If the material has a brown or violet color, then dissolve it in CHCl3, shake it with 5% sodium thiosulfate solution until is colourless. Dry (Na2SO4), extract, evaporate and disil the residue in vacuo. [Dains & Eberly Org Synth Coll Vol II 355 1948, Beilstein 6 IV 1074.]
4-Iodophenol Preparation Products And Raw materials
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