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Cyclobutanecarboxylic acid

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Cyclobutanecarboxylic acid Basic information
Cyclobutanecarboxylic acid Chemical Properties
Safety Information
MSDS
Cyclobutanecarboxylic acid Usage And Synthesis
  • Chemical PropertiesCLEAR COLOURLESS TO SLIGHTLY AMBER LIQUID
  • Synthesis Reference(s)The Journal of Organic Chemistry, 22, p. 1680, 1957 DOI: 10.1021/jo01363a041
  • Purification MethodsDissolve the acid in aqueous HCO 3 then acidify with HCl and extract it into Et2O, wash with H2O, dry (Na2SO4), concentrate to a small volume, then distil it through a glass helices packed column. The S-benzylisothiuronium salt has m 176o (from EtOH), the anilide has m 112.5-113o, and the p-toluide has m 123o. [Payne & Smith J Org Chem 22 1680 1957, Kantaro & Gunning J Am Chem Soc 73 480 1951, Stodola & Heisig Org Synth Coll Vol III 213 1955, Beilstein 9 H 5.]
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