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(-)-Camphanic acid chloride

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(-)-Camphanic acid chloride Basic information
(-)-Camphanic acid chloride Chemical Properties
  • Melting point:71-73 °C(lit.)
  • alpha -18 º (c=2, CCl4)
  • Boiling point:310.92°C (rough estimate)
  • Density 1.2072 (rough estimate)
  • refractive index 1.5390 (estimate)
  • storage temp. −20°C
  • form Powder
  • color Yellow to orange-brown
  • optical activity[α]23/D 18°, c = 2 in carbon tetrachloride
  • Water Solubility decomposes
  • Sensitive Moisture Sensitive
  • BRN 3590860
  • InChIKeyPAXWODJTHKJQDZ-RGURZIINSA-N
  • CAS DataBase Reference39637-74-6(CAS DataBase Reference)
Safety Information
  • Hazard Codes C,Xi
  • Risk Statements 34-29
  • Safety Statements 26-36/37/39-45-8-27
  • RIDADR UN 3261 8/PG 2
  • WGK Germany 3
  • 10-21
  • HazardClass 8
  • PackingGroup II
  • HS Code 29322090
MSDS
(-)-Camphanic acid chloride Usage And Synthesis
  • Chemical PropertiesOff-White Powder
  • UsesAn optically active resolving agent
  • Purification MethodsIt is soluble in toluene (50g/100mL at 0o) and crystallises from pet ether (b 40-60o). It sublimes at 70o/5mm, Store it dry at 0o, max (CCl4) 1805s and 1780m cm-1. Armarego et al. J Chem Soc, Perkin Trans I 2229 1976, Gerlach Helv Chim Acta 51 1587 1968, Gerlach Helv Chim Acta 68 1815 1985, Beilstein 18/8 V 101.]
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