喹啉,1,2,3,4-四氢-6-甲基喹啉

Mass

MS-KW-0532          
6-methyl-1,2,3,4-tetrahydroquinoline
C10H13N             (Mass of molecular ion:    147)

   Source Temperature: 190 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       1.5
      28.0       1.5
      39.0       3.6
      41.0       1.6
      50.0       1.1
      51.0       3.4
      52.0       1.9
      53.0       1.2
      58.5       3.9
      59.5       1.6
      63.0       2.6
      64.0       1.1
      64.5       1.6
      65.0       6.6
      65.5       3.3
      66.0       1.5
      70.5       1.2
      71.5       7.2
      72.0       2.8
      72.5       8.7
      73.0       2.0
      73.5       2.2
      77.0       4.9
      78.0       1.8
      79.0       1.6
      89.0       2.2
      90.0       1.4
      91.0       8.2
      92.0       1.8
     102.0       1.2
     103.0       2.7
     104.0       1.7
     105.0       2.3
     115.0       4.8
     116.0       1.9
     117.0      11.1
     118.0       7.3
     119.0       4.0
     120.0       1.2
     128.0       1.3
     129.0       2.0
     130.0      15.7
     131.0      19.7
     132.0      30.7
     133.0       3.1
     142.0       3.2
     143.0       6.0
     144.0       9.4
     145.0       3.7
     146.0      89.7
     147.0     100.0
     148.0      10.7

Assign. Shift(ppm) A 6.77 B 6.385 C 3.6 D 3.245 E 2.716 F 2.193 G 1.911

     Hz     ppm     Int.

   2707.89   6.774    126
   2707.28   6.772    124
   2701.67   6.758    271
   2556.65   6.396    220
   2553.59   6.388     40
   2551.27   6.382     51
   2548.10   6.374    202
   1457.52   3.646     20
   1302.50   3.258    230
   1300.18   3.253     76
   1297.00   3.245    241
   1293.95   3.237     75
   1291.51   3.231    240
   1092.29   2.733    142
   1085.82   2.717    262
   1079.35   2.700    156
    876.71   2.193   1000
    775.64   1.941     85
    773.44   1.935     29
    771.49   1.930     52
    769.05   1.924    170
    767.22   1.920     61
    764.78   1.913    144
    763.68   1.911    151
    762.58   1.908    156
    760.50   1.903     64
    758.06   1.897    159
    755.86   1.891     58
    753.91   1.886     29
    751.71   1.881     79