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MassMS-KW-0532 6-methyl-1,2,3,4-tetrahydroquinoline C10H13N (Mass of molecular ion: 147)
Source Temperature: 190 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 1.5 28.0 1.5 39.0 3.6 41.0 1.6 50.0 1.1 51.0 3.4 52.0 1.9 53.0 1.2 58.5 3.9 59.5 1.6 63.0 2.6 64.0 1.1 64.5 1.6 65.0 6.6 65.5 3.3 66.0 1.5 70.5 1.2 71.5 7.2 72.0 2.8 72.5 8.7 73.0 2.0 73.5 2.2 77.0 4.9 78.0 1.8 79.0 1.6 89.0 2.2 90.0 1.4 91.0 8.2 92.0 1.8 102.0 1.2 103.0 2.7 104.0 1.7 105.0 2.3 115.0 4.8 116.0 1.9 117.0 11.1 118.0 7.3 119.0 4.0 120.0 1.2 128.0 1.3 129.0 2.0 130.0 15.7 131.0 19.7 132.0 30.7 133.0 3.1 142.0 3.2 143.0 6.0 144.0 9.4 145.0 3.7 146.0 89.7 147.0 100.0 148.0 10.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C10H13N 0.034 g : 0.5 ml CDCl3 6-methyl-1,2,3,4-tetrahydroquinoline 
Assign. Shift(ppm)
A 6.77 B 6.385 C 3.6 D 3.245 E 2.716 F 2.193 G 1.911
Hz ppm Int.2707.89 6.774 126 2707.28 6.772 124 2701.67 6.758 271 2556.65 6.396 220 2553.59 6.388 40 2551.27 6.382 51 2548.10 6.374 202 1457.52 3.646 20 1302.50 3.258 230 1300.18 3.253 76 1297.00 3.245 241 1293.95 3.237 75 1291.51 3.231 240 1092.29 2.733 142 1085.82 2.717 262 1079.35 2.700 156 876.71 2.193 1000 775.64 1.941 85 773.44 1.935 29 771.49 1.930 52 769.05 1.924 170 767.22 1.920 61 764.78 1.913 144 763.68 1.911 151 762.58 1.908 156 760.50 1.903 64 758.06 1.897 159 755.86 1.891 58 753.91 1.886 29 751.71 1.881 79
in CDCl3
KBr disk
Nujol
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