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网站主页CAS数据库列表 91-61-2更多图谱喹啉,1,2,3,4-四氢-6-甲基喹啉(91-61-2)核磁图(1HNMR)

喹啉,1,2,3,4-四氢-6-甲基喹啉

产品名称 喹啉,1,2,3,4-四氢-6-甲基喹啉

CAS号91-61-2

分子式C10H13N

分子量147.22

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  • Mass

    MS-KW-0532          
    6-methyl-1,2,3,4-tetrahydroquinoline
    C10H13N             (Mass of molecular ion:    147)
    

       Source Temperature: 190 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       1.5
          28.0       1.5
          39.0       3.6
          41.0       1.6
          50.0       1.1
          51.0       3.4
          52.0       1.9
          53.0       1.2
          58.5       3.9
          59.5       1.6
          63.0       2.6
          64.0       1.1
          64.5       1.6
          65.0       6.6
          65.5       3.3
          66.0       1.5
          70.5       1.2
          71.5       7.2
          72.0       2.8
          72.5       8.7
          73.0       2.0
          73.5       2.2
          77.0       4.9
          78.0       1.8
          79.0       1.6
          89.0       2.2
          90.0       1.4
          91.0       8.2
          92.0       1.8
         102.0       1.2
         103.0       2.7
         104.0       1.7
         105.0       2.3
         115.0       4.8
         116.0       1.9
         117.0      11.1
         118.0       7.3
         119.0       4.0
         120.0       1.2
         128.0       1.3
         129.0       2.0
         130.0      15.7
         131.0      19.7
         132.0      30.7
         133.0       3.1
         142.0       3.2
         143.0       6.0
         144.0       9.4
         145.0       3.7
         146.0      89.7
         147.0     100.0
         148.0      10.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10H13N 0.034 g : 0.5 ml CDCl3
    6-methyl-1,2,3,4-tetrahydroquinoline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.77 B 6.385 C 3.6 D 3.245 E 2.716 F 2.193 G 1.911

         Hz     ppm     Int.
    

       2707.89   6.774    126
       2707.28   6.772    124
       2701.67   6.758    271
       2556.65   6.396    220
       2553.59   6.388     40
       2551.27   6.382     51
       2548.10   6.374    202
       1457.52   3.646     20
       1302.50   3.258    230
       1300.18   3.253     76
       1297.00   3.245    241
       1293.95   3.237     75
       1291.51   3.231    240
       1092.29   2.733    142
       1085.82   2.717    262
       1079.35   2.700    156
        876.71   2.193   1000
        775.64   1.941     85
        773.44   1.935     29
        771.49   1.930     52
        769.05   1.924    170
        767.22   1.920     61
        764.78   1.913    144
        763.68   1.911    151
        762.58   1.908    156
        760.50   1.903     64
        758.06   1.897    159
        755.86   1.891     58
        753.91   1.886     29
        751.71   1.881     79
    

in CDCl3



KBr disk



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