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网站主页CAS数据库列表 635-46-1更多图谱1,2,3,4-四氢喹啉(635-46-1)核磁图(1HNMR)

1,2,3,4-四氢喹啉

产品名称 1,2,3,4-四氢喹啉

CAS号635-46-1

分子式C9H11N

分子量133.19

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  • Mass

    MS-NW-0057          
    1,2,3,4-tetrahydroquinoline
    C9H11N              (Mass of molecular ion:    133)
    

       Source Temperature: 220 °C
       Sample Temperature:  55 °C
       Reservoir, 75 eV
    

          27.0       1.6
          28.0       1.1
          39.0       3.5
          50.0       2.3
          51.0       6.1
          52.0       2.5
          58.5       1.3
          63.0       2.3
          64.0       1.0
          64.5       2.5
          65.0       4.7
          65.5       4.3
          66.0       1.5
          66.5       2.0
          74.0       1.0
          75.0       1.1
          76.0       1.5
          77.0      10.1
          78.0       5.6
          79.0       3.0
          89.0       1.6
          90.0       2.2
          91.0       7.2
         102.0       1.8
         103.0       4.1
         104.0       7.4
         105.0       4.8
         106.0       2.1
         115.0       4.6
         116.0       1.2
         117.0      17.5
         118.0      20.6
         119.0       1.9
         129.0       1.2
         130.0      12.3
         131.0       4.1
         132.0     100.0
         133.0      84.4
         134.0       8.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H11 N 14.0 mg : 0.5 ml CDCl3
    1,2,3,4-tetrahydroquinoline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.95 B 6.94 C 6.598 D 6.464 E 3.80 F 3.288 G 2.757 J 1.936

         Hz     ppm     Int.
    

       2788.82   6.979    138
       2788.21   6.977    258
       2787.35   6.975    244
       2786.62   6.973    314
       2785.89   6.971    151
       2781.62   6.961    201
       2780.88   6.959    368
       2780.27   6.957    437
       2779.42   6.955    706
       2778.69   6.953    815
       2778.08   6.952    640
       2777.59   6.951    645
       2776.61   6.948    463
       2776.00   6.947    232
       2775.02   6.944    122
       2773.80   6.941    129
       2773.19   6.940    230
       2772.34   6.937    406
       2771.61   6.936    748
       2770.87   6.934    663
       2770.02   6.932    725
       2769.04   6.929    510
       2768.43   6.928    221
       2767.58   6.926     91
       2644.78   6.618    408
       2643.55   6.615    393
       2637.45   6.600    687
       2636.35   6.597    614
       2630.13   6.582    354
       2628.91   6.579    333
       2587.65   6.475    590
       2587.16   6.474    586
       2586.43   6.472    545
       2579.83   6.456    541
       2579.22   6.454    562
       2578.61   6.453    503
       1518.68   3.801     89
       1319.82   3.303    905
       1317.26   3.297    258
       1314.33   3.289    920
       1311.40   3.282    234
       1308.84   3.275    941
       1108.64   2.775    524
       1102.17   2.758   1000
       1099.00   2.750     92
       1095.83   2.742    607
        784.91   1.964    391
        782.59   1.959    111
        780.76   1.954    223
        779.30   1.950    465
        778.32   1.948    655
        776.37   1.943    222
        775.51   1.941    187
        773.80   1.937    595
        773.07   1.935    530
        772.71   1.934    557
        771.97   1.932    605
        769.65   1.926    216
        767.33   1.921    614
        765.14   1.915    195
        763.31   1.910     88
        760.99   1.905    350
    

in CDCl3



liquid film