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网站主页CAS数据库列表 90-41-5更多图谱邻氨基联苯(90-41-5)红外图谱(IR3)

邻氨基联苯

产品名称 邻氨基联苯

CAS号90-41-5

分子式C12H11N

分子量169.22

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  • Mass

    MS-NW-0169          
    2-biphenylylamine
    C12H11N             (Mass of molecular ion:    169)
    

       Source Temperature: 140 °C
       Sample Temperature:   0 °C
       Direct, 75 eV
    

          27.0       2.3
          28.0       3.2
          38.0       2.4
          39.0       8.1
          40.0       1.0
          41.0       1.8
          50.0       4.6
          51.0       7.3
          52.0       3.8
          54.0       1.0
          62.0       3.5
          63.0       7.7
          64.0       2.1
          65.0       3.5
          66.0       1.0
          70.5       1.5
          71.5       2.1
          74.0       3.3
          75.0       3.1
          76.0       3.1
          77.0       4.7
          78.0       1.3
          83.5       7.2
          84.0       1.5
          84.5       2.4
          86.0       1.5
          87.0       2.5
          88.0       1.5
          89.0       4.5
          90.0       2.2
          91.0       1.4
         102.0       2.5
         103.0       1.1
         113.0       1.7
         114.0       1.8
         115.0       9.2
         116.0       1.8
         117.0       1.1
         126.0       1.2
         127.0       1.6
         128.0       1.8
         130.0       1.0
         139.0       5.1
         140.0       3.2
         141.0       3.8
         142.0       1.2
         143.0       2.4
         151.0       1.1
         152.0       1.4
         154.0       3.2
         166.0       4.2
         167.0      24.4
         168.0      53.6
         169.0     100.0
         170.0      14.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H11 N 0.041 g : 0.5 ml CDCl3
    2-biphenylylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.43 B 7.33 C 7.14 D 7.117 E 6.813 F 6.735 G 3.71

         Hz     ppm     Int.
    

       2981.08   7.460     63
       2978.76   7.454    137
       2977.78   7.451     94
       2976.32   7.448     92
       2975.10   7.445     91
       2972.41   7.438   1000
       2970.58   7.433    549
       2969.24   7.430    215
       2966.06   7.422    375
       2965.33   7.420    469
       2963.26   7.415    133
       2959.35   7.405     87
       2958.25   7.403     93
       2957.28   7.400    132
       2956.18   7.397     40
       2935.30   7.345    108
       2933.23   7.340    157
       2930.54   7.333     95
       2929.32   7.330     94
       2928.22   7.327     83
       2927.37   7.325     91
       2926.51   7.323    154
       2924.93   7.319     80
       2923.71   7.316     69
       2922.36   7.313     54
       2920.29   7.308     79
       2917.85   7.302     51
       2861.57   7.161    111
       2859.99   7.157    143
       2854.25   7.142    153
       2853.76   7.141    143
       2852.66   7.138    213
       2852.17   7.137    207
       2849.00   7.129    215
       2848.63   7.128    216
       2847.41   7.125    186
       2846.92   7.124    167
       2846.44   7.123    152
       2844.85   7.119    212
       2841.43   7.110    234
       2841.06   7.109    241
       2839.84   7.106    181
       2730.47   6.833    158
       2729.25   6.830    176
       2723.02   6.814    239
       2721.92   6.811    250
       2715.58   6.795    131
       2714.36   6.792    141
       2696.04   6.747    218
       2695.56   6.745    207
       2694.82   6.743    216
       2688.11   6.727    202
       2687.62   6.725    200
       2687.01   6.724    199
       1484.38   3.715    151
    

in CDCl3



CCl4 solution



KBr disc



nujol mull



4880 A,200 M,powder