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MassMS-NW-0169 2-biphenylylamine C12H11N (Mass of molecular ion: 169)
Source Temperature: 140 °C Sample Temperature: 0 °C Direct, 75 eV
27.0 2.3 28.0 3.2 38.0 2.4 39.0 8.1 40.0 1.0 41.0 1.8 50.0 4.6 51.0 7.3 52.0 3.8 54.0 1.0 62.0 3.5 63.0 7.7 64.0 2.1 65.0 3.5 66.0 1.0 70.5 1.5 71.5 2.1 74.0 3.3 75.0 3.1 76.0 3.1 77.0 4.7 78.0 1.3 83.5 7.2 84.0 1.5 84.5 2.4 86.0 1.5 87.0 2.5 88.0 1.5 89.0 4.5 90.0 2.2 91.0 1.4 102.0 2.5 103.0 1.1 113.0 1.7 114.0 1.8 115.0 9.2 116.0 1.8 117.0 1.1 126.0 1.2 127.0 1.6 128.0 1.8 130.0 1.0 139.0 5.1 140.0 3.2 141.0 3.8 142.0 1.2 143.0 2.4 151.0 1.1 152.0 1.4 154.0 3.2 166.0 4.2 167.0 24.4 168.0 53.6 169.0 100.0 170.0 14.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H11 N 0.041 g : 0.5 ml CDCl3 2-biphenylylamine 
Assign. Shift(ppm)
A 7.43 B 7.33 C 7.14 D 7.117 E 6.813 F 6.735 G 3.71
Hz ppm Int.2981.08 7.460 63 2978.76 7.454 137 2977.78 7.451 94 2976.32 7.448 92 2975.10 7.445 91 2972.41 7.438 1000 2970.58 7.433 549 2969.24 7.430 215 2966.06 7.422 375 2965.33 7.420 469 2963.26 7.415 133 2959.35 7.405 87 2958.25 7.403 93 2957.28 7.400 132 2956.18 7.397 40 2935.30 7.345 108 2933.23 7.340 157 2930.54 7.333 95 2929.32 7.330 94 2928.22 7.327 83 2927.37 7.325 91 2926.51 7.323 154 2924.93 7.319 80 2923.71 7.316 69 2922.36 7.313 54 2920.29 7.308 79 2917.85 7.302 51 2861.57 7.161 111 2859.99 7.157 143 2854.25 7.142 153 2853.76 7.141 143 2852.66 7.138 213 2852.17 7.137 207 2849.00 7.129 215 2848.63 7.128 216 2847.41 7.125 186 2846.92 7.124 167 2846.44 7.123 152 2844.85 7.119 212 2841.43 7.110 234 2841.06 7.109 241 2839.84 7.106 181 2730.47 6.833 158 2729.25 6.830 176 2723.02 6.814 239 2721.92 6.811 250 2715.58 6.795 131 2714.36 6.792 141 2696.04 6.747 218 2695.56 6.745 207 2694.82 6.743 216 2688.11 6.727 202 2687.62 6.725 200 2687.01 6.724 199 1484.38 3.715 151
in CDCl3
CCl4 solution
KBr disc
nujol mull
4880 A,200 M,powder
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