-
MassMS-NW-0675 N-phenyl-1-naphthylamine C16H13N (Mass of molecular ion: 219)
Source Temperature: 170 °C Sample Temperature: 120 °C Direct, 75 eV
39.0 1.9 50.0 1.1 51.0 3.7 63.0 2.0 65.0 1.3 75.0 1.5 77.0 3.7 89.0 1.7 94.5 1.9 95.5 3.1 96.5 1.8 101.0 1.3 102.0 3.2 107.0 1.8 107.5 1.1 108.0 1.4 108.5 18.9 109.0 5.6 109.5 6.9 110.0 1.3 115.0 8.5 116.0 3.2 126.0 2.0 127.0 3.3 128.0 1.2 140.0 1.3 153.0 1.9 165.0 1.1 189.0 2.0 190.0 1.5 191.0 1.5 204.0 3.1 215.0 1.3 216.0 7.4 217.0 31.4 218.0 42.1 219.0 100.0 220.0 17.3 221.0 1.4
400 MHz in CDCl3
-
1H NMR 399.65 MHz C16 H13 N 0.050 g : 0.5 ml CDCl3 N-phenyl-1-naphthylamine 
Assign. Shift(ppm)
A 7.958 B 7.821 C 7.526 D 7.45 E 7.42 F 7.340 G 7.33 J 7.216 K 6.936 L 6.882 M 5.84 ASSIGNED BY H-H AND C-H COSY.
Hz ppm Int.3184.81 7.969 334 3176.64 7.949 368 3130.25 7.833 313 3128.91 7.830 342 3121.46 7.811 367 3011.35 7.535 288 3004.03 7.517 344 2996.58 7.499 35 2996.09 7.497 34 2986.33 7.473 148 2985.11 7.470 170 2979.49 7.456 339 2978.39 7.453 351 2971.80 7.437 370 2970.09 7.432 534 2968.38 7.428 370 2961.67 7.411 352 2960.45 7.408 313 2954.96 7.394 164 2953.61 7.391 148 2949.46 7.381 38 2944.46 7.368 207 2937.01 7.349 565 2929.57 7.331 1000 2927.73 7.326 659 2922.00 7.312 190 2920.29 7.308 129 2892.33 7.238 407 2884.77 7.219 694 2883.91 7.217 714 2876.46 7.198 522 2775.63 6.946 775 2767.94 6.926 667 2757.20 6.900 264 2749.88 6.881 433 2742.55 6.863 209 2334.23 5.841 258
in CDCl3
CCl4 solution
KBr disc
nujol mull
更多供应商
