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网站主页CAS数据库列表 134-32-7更多图谱1-萘胺(134-32-7)核磁图(13CNMR)

1-萘胺

产品名称 1-萘胺

CAS号134-32-7

分子式C10H9N

分子量143.19

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  • Mass

    MS-NW-8709          
    1-naphthylamine
    C10H9N              (Mass of molecular ion:    143)
    

       Source Temperature: 260 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          39.0       2.1
          50.0       1.1
          51.0       1.6
          57.5       2.2
          58.5       4.1
          62.0       1.4
          63.0       3.2
          65.0       1.7
          70.5       4.8
          71.5       7.8
          74.0       1.1
          75.0       1.2
          76.0       1.1
          77.0       1.4
          88.0       1.1
          89.0       3.8
          90.0       1.1
         113.0       1.6
         114.0       2.4
         115.0      31.0
         116.0      17.9
         117.0       3.2
         126.0       1.3
         140.0       2.0
         141.0       1.0
         142.0       5.3
         143.0     100.0
         144.0      11.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H9 N 0.041 g : 0.5 ml CDCl3
    1-naphthylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.77 B 7.75 C *1 7.43 D *1 7.40 E 7.290 F 7.261 G 6.716 J 4.04

         Hz     ppm     Int.
    

       3115.72   7.797     34
       3111.45   7.786    278
       3109.01   7.780    316
       3107.06   7.775     61
       3105.47   7.771    173
       3103.15   7.765    527
       3102.05   7.762    584
       3100.22   7.758    157
       3099.24   7.755    138
       3095.83   7.747    292
       3094.12   7.743    236
       3093.38   7.741    328
       3089.48   7.731     37
       3088.87   7.729     36
       2976.81   7.449     93
       2975.10   7.445    158
       2969.97   7.432    437
       2968.26   7.428    384
       2966.55   7.423    490
       2963.50   7.416   1000
       2960.45   7.408    409
       2958.62   7.404    386
       2956.79   7.399    418
       2951.78   7.386    149
       2949.95   7.382     96
       2921.02   7.309    108
       2919.56   7.306    165
       2919.19   7.305    154
       2911.62   7.286    499
       2910.89   7.284    438
       2907.47   7.276    818
       2904.66   7.269     30
       2900.51   7.258    734
       2899.29   7.255    259
       2892.33   7.238    294
       2688.35   6.727    475
       2686.89   6.724    463
       2681.52   6.710    464
       2679.93   6.706    464
       1615.48   4.043    112
    

in CDCl3



CCl4 solution



KBr disc



nujol mull



4880 A,200 M,powder