N,N-二乙基氯甲酰胺

Mass

MS-NW-3733          
N,N-diethylcarbamoyl chloride
C5H10ClNO           (Mass of molecular ion:    135)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      14.0       1.5
      15.0      11.6
      18.0       2.4
      26.0       7.2
      27.0      39.2
      28.0      21.6
      29.0     100.0
      30.0       5.4
      36.0       2.8
      39.0       1.4
      40.0       3.6
      41.0       6.7
      42.0      22.4
      43.0       2.1
      44.0      42.4
      45.0       1.0
      49.0       2.9
      51.0       1.1
      54.0       1.8
      55.0       1.4
      56.0      53.9
      57.0       2.5
      58.0       5.1
      63.0      15.1
      64.0      11.0
      65.0       5.3
      66.0       3.5
      70.0       8.5
      71.0       2.9
      72.0      77.1
      73.0       3.5
      78.0       2.5
      84.0       1.2
      92.0      43.0
      93.0       1.3
      94.0      14.0
     100.0      84.4
     101.0       5.3
     106.0       3.5
     108.0       1.4
     120.0      70.5
     121.0       3.8
     122.0      22.7
     123.0       1.2
     135.0      45.1
     136.0       3.1
     137.0      14.6
     139.0       1.1
     172.0       1.7

Assign. Shift(ppm) A *1 3.46 B *1 3.44 C 1.23

     Hz     ppm     Int.

    322.69   3.604     75
    316.00   3.529    250
    309.25   3.453    366
    302.88   3.382    280
    298.31   3.331     78
    297.88   3.327     78
    296.13   3.307     94
    295.81   3.303     94
    116.88   1.306    558
    109.75   1.226   1000
    102.56   1.146    474
     96.69   1.080     26