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MS-NW-3733 N,N-diethylcarbamoyl chloride C5H10ClNO (Mass of molecular ion: 135)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
14.0 1.5 15.0 11.6 18.0 2.4 26.0 7.2 27.0 39.2 28.0 21.6 29.0 100.0 30.0 5.4 36.0 2.8 39.0 1.4 40.0 3.6 41.0 6.7 42.0 22.4 43.0 2.1 44.0 42.4 45.0 1.0 49.0 2.9 51.0 1.1 54.0 1.8 55.0 1.4 56.0 53.9 57.0 2.5 58.0 5.1 63.0 15.1 64.0 11.0 65.0 5.3 66.0 3.5 70.0 8.5 71.0 2.9 72.0 77.1 73.0 3.5 78.0 2.5 84.0 1.2 92.0 43.0 93.0 1.3 94.0 14.0 100.0 84.4 101.0 5.3 106.0 3.5 108.0 1.4 120.0 70.5 121.0 3.8 122.0 22.7 123.0 1.2 135.0 45.1 136.0 3.1 137.0 14.6 139.0 1.1 172.0 1.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H10 Cl N O 0.04 ml : 0.5 ml CDCl3 N,N-diethylcarbamoyl chloride Assign. Shift(ppm)
A *1 3.46 B *1 3.44 C 1.23
Hz ppm Int.
322.69 3.604 75 316.00 3.529 250 309.25 3.453 366 302.88 3.382 280 298.31 3.331 78 297.88 3.327 78 296.13 3.307 94 295.81 3.303 94 116.88 1.306 558 109.75 1.226 1000 102.56 1.146 474 96.69 1.080 26
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