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MassMS-NW-1137 N,N-diethylhydroxylamine C4H11NO (Mass of molecular ion: 89)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
14.0 1.7 15.0 18.4 17.0 7.3 18.0 35.8 19.0 6.9 26.0 10.8 27.0 51.8 28.0 64.9 29.0 100.0 30.0 62.9 31.0 1.6 32.0 1.7 38.0 1.0 39.0 2.7 40.0 5.3 41.0 30.7 42.0 58.9 43.0 6.2 44.0 27.7 45.0 3.8 46.0 67.0 47.0 1.2 52.0 1.2 54.0 3.8 55.0 6.4 56.0 51.9 57.0 3.8 58.0 71.3 59.0 21.0 60.0 8.7 68.0 1.6 69.0 1.6 70.0 10.3 71.0 12.7 72.0 15.0 73.0 18.6 74.0 76.6 75.0 3.0 87.0 41.9 88.0 10.1 89.0 23.8 90.0 1.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C4 H11 N O 0.04 ml : 0.5 ml CDCl3 N,N-diethylhydroxylamine 
Assign. Shift(ppm)
A 7. B 2.723 C 1.154
Hz ppm Int.255.13 2.849 74 248.06 2.770 295 240.94 2.691 337 234.06 2.614 111 110.19 1.231 427 103.13 1.152 1000 95.94 1.072 337
in CDCl3
liquid film
4880 A,200 M,liquid
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