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MS-NW-1439 3-chloro-o-toluidine C7H8ClN (Mass of molecular ion: 141)
Source Temperature: 240 °C Sample Temperature: 180 °C Reservoir, 75 eV
18.0 1.2 27.0 2.4 28.0 4.5 30.0 4.3 37.0 1.1 38.0 1.9 39.0 4.4 41.0 1.3 42.0 2.2 50.0 4.7 51.0 9.7 51.5 2.1 52.0 6.6 52.5 8.9 53.0 3.3 54.0 1.7 61.0 1.0 62.0 1.6 63.0 3.5 65.0 1.6 70.5 2.3 73.0 1.2 74.0 1.5 75.0 2.2 76.0 1.8 77.0 18.8 78.0 7.3 79.0 8.9 80.0 1.5 89.0 7.5 90.0 1.0 104.0 7.4 105.0 3.2 106.0 72.5 107.0 5.9 113.0 1.8 124.0 2.0 140.0 32.0 141.0 100.0 142.0 17.2 143.0 31.7 144.0 2.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H8 Cl N 0.02 ml : 0.5 ml CDCl3 3-chloro-o-toluidine Assign. Shift(ppm)
A 6.93 B 6.78 C 6.55 D 3.57 E 2.200
Hz ppm Int.
620.31 6.927 99 619.88 6.922 97 612.69 6.842 182 611.94 6.833 151 609.69 6.808 208 603.69 6.741 55 590.00 6.588 109 588.06 6.567 102 583.25 6.513 55 582.75 6.507 62 580.81 6.486 63 324.88 3.628 33 323.69 3.615 43 320.25 3.576 85 319.63 3.569 85 318.69 3.559 81 315.63 3.525 42 315.31 3.521 41 314.81 3.516 37 197.00 2.200 1000
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